4'-Nitroacetanilide
4'-Nitroacetanilide
CAS: 104-04-1
Molecular Formula: C8H8N2O3
4'-Nitroacetanilide - Names and Identifiers
| Name | 4'-Nitroacetanilide |
| Synonyms | 104-04-1 P-NITROACETANILIDE p-nitro-acetanilid 4'-Nitroacetanilide LABOTEST-BB LT00455738 N-ACETYL-4-NITROANILINE p-Nitrophenylacetanilide N-(4-Nitrophenyl)acetamide N1-(4-nitrophenyl)acetamide Acetamide, N-(4-nitrophenyl)- 4μ-Nitroacetanilide, Acetic acid 4-nitroanilide |
| CAS | 104-04-1 |
| EINECS | 203-169-0 |
| InChI | InChI=1/C8H8N2O3/c1-6(11)9-7-2-4-8(5-3-7)10(12)13/h2-5H,1H3,(H,9,11) |
4'-Nitroacetanilide - Physico-chemical Properties
| Molecular Formula | C8H8N2O3 |
| Molar Mass | 180.16 |
| Density | 1.340 |
| Melting Point | 213-215°C(lit.) |
| Boling Point | 312.97°C (rough estimate) |
| Flash Point | 201.1°C |
| Water Solubility | 2.2g/L(room temperature) |
| Solubility | 2.2g/l |
| Vapor Presure | 6.77E-07mmHg at 25°C |
| Appearance | Yellow to tan powder |
| Color | Yellow to green-yellow or green-brown |
| Merck | 14,6581 |
| BRN | 2211962 |
| pKa | 13.91±0.70(Predicted) |
| Storage Condition | Store below +30°C. |
| Stability | Stable. Combustible. Incompatible with strong oxidizing agents. |
| Refractive Index | 1.6180 (estimate) |
| MDL | MFCD00007303 |
| Physical and Chemical Properties | White prismatic crystals. Melting point 215-216(207 °c), boiling point 100 °c (1.06 x 10-3kPa). Soluble in hot water, alcohol, ether, soluble in potassium hydroxide solution into orange, almost insoluble in cold water. |
4'-Nitroacetanilide - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
| RTECS | AE5075000 |
| TSCA | Yes |
| HS Code | 29242990 |
4'-Nitroacetanilide - Reference Information
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| use | as an intermediate for drugs and dyes. |
| production method | prepared by nitration of acetanilide. 675kg of 98% sulfuric acid was added into a nitrification pot, stirred, and 225kg of 99% acetanilide was added within 20-25 ℃ for 2-2.5h hours. After all dissolution, the temperature is reduced to 7 ℃, and mixed acid (made of 63kg of water, 60kg of 98% sulfuric acid and 107kg of 96% nitric acid) is added dropwise within about 20h at 4-7 ℃. After dropping, dilute in 4000L ice water and let stand for 1h. Siphon separates the upper waste acid, filters the lower material, and washes it to neutral to obtain 4-nitroacetanilide. Another preparation method is obtained by acetylation of p-nitroaniline. |
Last Update：2024-04-09 21:04:16
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