(3S)-3-amino-1-benzyl-azepan-2-one

(3S)-3-amino-1-benzyl-azepan-2-one - Names and Identifiers

Name	(3S)-3-amino-1-benzyl-azepan-2-one
Synonyms	L--Amino--N-benzyl-caprolactam (S)-3-Amino-1-benzylazepan-2-one L-A-AMINO-E-N-BENZYL-CAPROLACTAM (3S)-3-Amino-1-benzylazepan-2-one (3S)-3-amino-1-benzyl-azepan-2-one (3S)-3-Amino-1-benzyl-azepan-2-one L-alpha-Amino-epsilon-N-benzyl-caprolactam (3S)-3-Aminohexahydro-1-benzyl-2H-azepin-2-one 2H-Azepin-2-one, 3-aminohexahydro-1-(phenylmethyl)-, (3S)-
CAS	209983-91-5
InChI	InChI=1/C13H18N2O/c14-12-8-4-5-9-15(13(12)16)10-11-6-2-1-3-7-11/h1-3,6-7,12H,4-5,8-10,14H2/t12-/m0/s1

(3S)-3-amino-1-benzyl-azepan-2-one - Physico-chemical Properties

Molecular Formula	C13H18N2O
Molar Mass	218.29
Density	1.104
Boling Point	405℃
Flash Point	199℃
Vapor Presure	9.35E-07mmHg at 25°C
Storage Condition	2-8°C
Refractive Index	1.561

(3S)-3-amino-1-benzyl-azepan-2-one - Introduction

(3S)-is an organic compound with the following properties:

1. Appearance: usually white or white crystal powder.

2. Solubility: soluble in some polar solvents, such as methanol, ethanol and chloroform.

3. Stability: It is relatively stable at room temperature, but it will decompose at high temperature, sunlight and in the presence of strong oxidants.

(3S)-The main use of the compound is as a chemical reagent and intermediate. It can be used in organic synthesis reactions, such as the synthesis of chiral compounds and drugs. Because of its chiral structure, it has important application value in the preparation and study of enantiomers.

The method of preparing (3S)-is comprised of the following steps:

1. Dissolve benzylamine in a suitable solvent, such as methanol or ethanol.

2. Add an appropriate amount of sodium hydroxide (NaOH) Dropwise to the solution and maintain the temperature.

3. Add chloroformate reagent, such as benzyl chloroformate (methyl chloroformate).

4. Continue stirring and reaction until the reaction is complete.

5. Crystallization or purification is carried out to obtain (3S)-is.

Safety precautions when using and handling (3S):

1. Avoid contact with skin, eyes and respiratory tract. Wear protective gloves, glasses and masks as necessary.

2. In operation and storage, should be away from the fire and high temperature, high pressure environment.

3. Take care to follow proper operating procedures and laboratory safety regulations.

4. If contact occurs, flush the affected area immediately with plenty of water and seek medical help.

Please make sure to follow the appropriate safety instructions when using this compound, and consult a professional if necessary.

Last Update：2024-04-09 21:21:28