2,3-二氯-4-碘吡啶 - Names and Identifiers
2,3-二氯-4-碘吡啶 - Physico-chemical Properties
Molecular Formula | C5H2Cl2IN
|
Molar Mass | 273.89 |
Density | 2.129±0.06 g/cm3(Predicted) |
Melting Point | 109-113°C |
Boling Point | 284.3±35.0 °C(Predicted) |
pKa | -0.80±0.10(Predicted) |
Storage Condition | under inert gas (nitrogen or Argon) at 2–8 °C |
2,3-二氯-4-碘吡啶 - Risk and Safety
Hazard Symbols | Xn - Harmful

|
Risk Codes | R22 - Harmful if swallowed
R36 - Irritating to the eyes
|
Safety Description | 26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
|
UN IDs | 2811 |
WGK Germany | 3 |
Hazard Class | IRRITANT |
Packing Group | Ⅲ |
2,3-二氯-4-碘吡啶 - Introduction
Pyridine, 2,3-dichloro-4-iodo-is an organic compound with the chemical structure of C5HCl2IN. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
-Appearance: Pyridine, 2,3-dichloro-4-iodo-is colorless to slightly yellow crystal or powder
-Solubility: Soluble in ketones, ethanol and acetonitrile, insoluble in water
-Melting point and boiling point: its melting point is about 105-107 ℃, and its boiling point is about 273-274 ℃
-Flammability: The compound has low combustibility
Use:
Pyridine, 2,3-dichloro-4-iodo-can be used for different reaction types in organic synthesis, such:
-Catalyst: It can be used as a ligand of the complex to participate in the synthesis of metal catalysts.
-Reagent: It can be used as a reagent for the synthesis of β-bromoketones from 1,4-dipyridyl carbonitrile and α-halogenated ketones.
Preparation Method:
A method for synthesizing Pyridine, 2,3-dichloro-4-iodo-is as follows:
2,3-dichloro-4-methylpyridine is reacted with iodine in an appropriate organic solvent, usually using sodium iodide as a catalyst. The reaction is generally carried out at room temperature, and the reaction time may be increased or the reaction solution may be heated as required.
Safety Information:
Note the following when using and handling Pyridine, 2,3-dichloro-4-iodo:
-The compound is irritating to eyes and skin, avoid contact with skin and eyes.
-When in contact with strong oxidants and strong acids, harmful gases may be generated.
-Appropriate protective measures such as gloves, goggles and protective clothing should be taken during use and handling.
-Good ventilation must be maintained during laboratory operations.
-Waste to be disposed of in accordance with local regulations.
Last Update:2024-04-09 19:05:52