3-Pyridinol, 2-bromo-6-iodo- - Names and Identifiers
3-Pyridinol, 2-bromo-6-iodo- - Physico-chemical Properties
Molecular Formula | C5H3BrINO
|
Molar Mass | 299.89 |
Density | 2.512±0.06 g/cm3(Predicted) |
Melting Point | 141-142 °C(Solv: chloroform (67-66-3)) |
Boling Point | 404.0±45.0 °C(Predicted) |
pKa | 3.96±0.10(Predicted) |
Storage Condition | under inert gas (nitrogen or Argon) at 2–8 °C |
3-Pyridinol, 2-bromo-6-iodo- - Risk and Safety
Hazard Symbols | Xn - Harmful
|
Risk Codes | 22 - Harmful if swallowed
|
WGK Germany | 3 |
Hazard Class | IRRITANT |
3-Pyridinol, 2-bromo-6-iodo- - Upstream Downstream Industry
3-Pyridinol, 2-bromo-6-iodo- - Introduction
It is an organic compound with the chemical formula C5H3BrIN. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
-Appearance: It is a colorless to yellowish crystal.
-Solubility: It has limited miscibility in water and is soluble in organic solvents such as ethanol and dimethyl sulfoxide.
-Melting point: Its melting point is about 94-96 ° C.
Use:
Ti is often used as a starting material and intermediate in organic synthesis for the synthesis of other compounds. It has a wide range of applications in the fields of metal organic chemistry and material science.
Method:
The preparation of Lin can be carried out by the following steps:
1. Obtain 3,5-dibromopyridine.
2. Under alkaline conditions, 3,5-dibromopyridine reacts with potassium hydroxide (KOH) to generate 3-Bromopyridine (3-Bromopyridine).
3. 3-bromopyridine reacts with potassium hydroxide and hydrogen hydroxide to generate 2-Bromo-3-hydroxypyridine (2-Bromo-3-hydroxypyridine).
4. Finally, 2-bromo-3-hydroxypyridine is reacted with sodium iodide (NaI) to obtain the target product.
Safety Information:
must comply with laboratory safety procedures for handling. Since this is an organic compound, it may be potentially harmful to the human body. Therefore, it is necessary to take appropriate protective measures during use and storage, such as wearing gloves, goggles and laboratory coats. In addition, maintain a well-ventilated working environment and avoid exposure to high temperatures, fire sources and strong acids.
Last Update:2024-04-10 22:29:15