Name | 4'-Bromoacetanilide |
Synonyms | Asepsin Bromanilide Bromoanalide Bromcantifebrin Bromoantifebrin Bromoacetanilide Bromoacetoanilide 4-Bromoacetanilide Acet-p-bromoanilide 4'-Bromoacetanilide 4-Bromoacetoanilide Aceto-p-bromoanilide N-(4-Bromophenyl)acetamide |
CAS | 103-88-8 |
EINECS | 203-154-9 |
InChI | InChI=1/C8H8BrNO/c1-6(11)10-8-4-2-7(9)3-5-8/h2-5H,1H3,(H,10,11) |
Molecular Formula | C8H8BrNO |
Molar Mass | 214.06 |
Density | 1.72 |
Melting Point | 165-169°C(lit.) |
Boling Point | 353.4°C (estimate) |
Flash Point | 167.6°C |
Water Solubility | Insoluble |
Solubility | alcohol: moderately soluble |
Vapor Presure | 3.58E-05mmHg at 25°C |
Appearance | White to light brown crystals |
Color | White to beige or light gray |
Merck | 14,1399 |
BRN | 2208091 |
pKa | 14.25±0.70(Predicted) |
Storage Condition | Store below +30°C. |
Stability | Stable. Incompatible with strong oxidizing agents. |
Refractive Index | 1.6120 (estimate) |
MDL | MFCD00000092 |
Physical and Chemical Properties | Light yellow crystals or powdery crystals. Melting point 168 ℃, relative density 1.717. Soluble in benzene, chloroform, ethyl acetate, slightly soluble in alcohol, slightly soluble in hot water, insoluble in cold water. |
Hazard Symbols | Xi - Irritant |
Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
UN IDs | 2811 |
WGK Germany | 3 |
RTECS | AD9625000 |
TSCA | Yes |
HS Code | 29242998 |
Hazard Note | Irritant |
Hazard Class | 6.1(b) |
Packing Group | III |
chemical properties | light yellow crystal or powdery crystal. Melting point 168 ℃, relative density 1.717. Soluble in benzene, chloroform, ethyl acetate, slightly soluble in alcohol, slightly soluble in hot water, insoluble in cold water. |
use | organic synthesis intermediate. |
production method | is obtained by bromination of acetanilide. Dissolve acetanilide in ethanol, cool to about 10 ℃, slowly add bromine, control the temperature at 20-25 ℃, add it for about 1.5-2h, stir for 0.5h, leave it for one day, then pour it into sodium bisulfite solution, filter, wash with water, and recrystallize with ethanol to obtain the finished product. |
NIST chemical information | The information is: webbook.nist.gov provides (external link) |
EPA chemical information | The information is: offered by ofmpub.epa.gov (external link) |