Name | Poly(ethylene glycol) distearate |
Synonyms | Polyethyleneglycol3distearate Poly(ethylene glycol) distearate |
CAS | 9005-08-7 |
Molecular Formula | (C2H4O)n.C36H70O3 |
Molar Mass | 332.518 |
Melting Point | 35-37 °C |
Flash Point | >230 °F |
Storage Condition | Room Temprature |
Physical and Chemical Properties | Chemical nature of this product is a white solid, soluble in isopropanol, glycerol, gasoline solvent, dispersed in water, melting point 35~37 ℃. |
Use | This product is used as an emulsifier and thickener in cosmetics and detergent industry, and can also be used as a plasticizer for various resins, as a water removing component of grinding paste and polishing paste. |
Author:
Abstract:
polyethylene glycol distearate was synthesized by using phosphorous acid and sulfuric acid composite catalyst. The optimum process conditions were: n acid: n alcohol 2.8:1(mol:mol), the dosage of composite catalyst was 1.0% (based on polyethylene glycol), the reaction temperature was 150 ℃, the reaction time was 5h, and the vacuum degree was 97.3kPa.
Key words:
polyethylene glycol stearate surfactant synthesis Non-ionic
DOI:
CNKI:SUN:JSHG.0.1997-06-007
cited:
year:
1997
Abstract:
Polyethylene glycol distearate was prepared by transesterification under normal pressure with polyethylene glycol (6000) and monoglyceride Stearate as raw materials and p-toluenesulfonic acid as catalyst. The optimum reaction conditions were determined by orthogonal experiment. Combined with the experimental principle and method, the effects of catalyst, reaction temperature, reaction time and material ratio on the reaction were discussed, the viscosity of polyethylene glycol distearate solution with different concentrations was measured. The optimum conditions for the synthesis reaction are as follows: the amount of catalyst is 2%(molar ratio), the reaction temperature is 130 ℃, the time is 4H, and n (stearate):n (polyethylene glycol) = 4:1. Under these conditions, the yield was 98%.Key words:
transesterification method polyethylene glycol (6000) stearic acid monoglyceride polyethylene glycol distearate thickener
DOI:
10.3969/j.issn.1672-2701.2008.03.019
cited:
year:
2008
Author:
Abstract:
polyethylene glycol distearate was prepared by the esterification reaction of low molecular weight polyethylene glycol and acyl chloride stearic acid by emulsion method, the core-shell structure materials with phase transition function were prepared. The esterification products and core-shell structure materials were characterized by FT-IR,DSC,TG and polarized light microscopy. The solid-liquid phase transition temperature of PEG200 distearate is 30 ℃ ~ 35 ℃, and the phase transition enthalpy is 95J/g. The enthalpy of phase transition of core-shell material is 32J/g.
Key words:
esterification reaction core-shell structure solid-liquid phase transition enthalpy of phase change
DOI:
10.3321/j.issn:1000-7555.2007.02.045
cited:
year:
2007
Abstract:
Polyethylene glycol distearate was prepared by transesterification under normal pressure with polyethylene glycol (6000), stearic acid monoglyceride as basic raw material and p-toluenesulfonic acid as catalyst. The optimum reaction conditions were determined by orthogonal experiment. Combined with the experimental principle and method, the effects of catalyst, reaction temperature, reaction time and material ratio on the reaction were discussed, the viscosity of polyethylene glycol distearate solution with different concentrations was measured. The research shows that the optimum conditions for the synthesis reaction are as follows: the amount of catalyst is 2 (molar ratio), the reaction temperature is 130 ℃, the time is 4H, n...Key words:
transesterification method polyethylene glycol stearic acid monoglyceride polyethylene glycol distearate thickener synthesis reaction
meeting name:
The 90th academic conference of fine chemical engineering committee of China Chemical Society and the 13th National Conference on Research and development of industrial surfactants
Meeting Time:
2006-08-01
cited:
Author:
Zhao Shan Cui , Wang Baoqi , Jiang Chuan , Guo Yanling
Abstract:
Amphiphilic polyethylene glycol distearate was synthesized and characterized by IR and NMR. Using pyrene as a model drug, the critical micelle concentration of polymer micelles was determined by fluorescence probe method, and the critical micelle concentration was 3.98 × 10 ~(-2) g/L(1.53 × 10 ~(-5)). mol/L). Lutein was embedded with polyethylene glycol distearate as carrier, and lutein-loaded polymeric micelles were prepared by solvent evaporation method. The results of dynamic light scattering showed that the micelles were monodisperse and the average particle size was 180 nm. Atomic force microscopy showed that the prepared micelles were generally spherical and uniform in size. The drug loading rate of lutein in the drug loaded micelles was 10.36%, and it had good water solubility.Key words:
lutein polyethylene glycol distearate micelles water-soluble
meeting name:
National Annual Meeting of Applied Chemistry, Chinese Chemical Society
Meeting Time:
2011
cited:
invention patent
Application (patent) number:
CN201310312094.1
application date:
20130724
Public/Announcement Number:
CN103410002A
Public/announcement date:
20131127
applicant (patent):
Yadi knitting garment factory, Miaogang, Qidu town, Wujiang City
inventor:
National and provincial code:
CN320509
Abstract:
A wool garment treatment agent containing polyethylene glycol distearate, which consists of the following components in a weight ratio: polyethylene glycol distearate 5-10 parts, polyglycerol fatty acid ester 3-5 parts, magnesium sulfate 4-9 parts, propylene glycol 5-10 parts, ethyl cellulose 1-3 parts, water 400-500 parts. The prepared wool knitting agent has good anti-Pilling function.