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AKOS BBS-00003909

Phenylacetyl chloride

CAS: 103-80-0

Molecular Formula: C8H7ClO

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AKOS BBS-00003909 - Names and Identifiers

Name Phenylacetyl chloride
Synonyms phenylacetyl
-Toluylchloride
A-TOLUYL CHLORIDE
AKOS BBS-00003909
Phenacetyl chloride
Phenylacetyl chloride
alpha-Toluyl chloride
Phenylacethylchloride
Phenyl acetyl chloride
Benzeneacetyl chloride
LABOTEST-BB LT00643802
Acetyl chloride, phenyl-
Phenylacetic acid chloride
alpha-Phenylacetyl chloride
CAS 103-80-0
EINECS 203-146-5
InChI InChI=1/C8H7ClO/c9-8(10)6-7-4-2-1-3-5-7/h1-5H,6H2

AKOS BBS-00003909 - Physico-chemical Properties

Molecular FormulaC8H7ClO
Molar Mass154.59
Density1.169 g/mL at 25 °C (lit.)
Melting Point264-266 °C(Solv: N,N-dimethylformamide (68-12-2))
Boling Point94-95 °C/12 mmHg (lit.)
Flash Point217°F
Solubility Miscible with alcohol and ether.
Vapor Presure0.124mmHg at 25°C
Appearanceclear liquid
ColorColorless to Light yellow
BRN742254
Storage Condition2-8°C
StabilityStable. Reacts with water. Incompatible with amines, most common metals, moisture, strong oxidizing agents.
SensitiveMoisture Sensitive
Refractive Indexn20/D 1.5325(lit.)
Physical and Chemical PropertiesDensity 1.16
boiling point 94-95 ° C (12 torr)
refractive index 533-1.102
flash point ° C
UseUsed as pharmaceutical, pesticide, Fragrance Intermediates

AKOS BBS-00003909 - Risk and Safety

Hazard SymbolsC - Corrosive
Corrosive
Risk CodesR34 - Causes burns
R37 - Irritating to the respiratory system
R14 - Reacts violently with water
Safety DescriptionS26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection.
S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S25 - Avoid contact with eyes.
S27 - Take off immediately all contaminated clothing.
UN IDsUN 2577 8/PG 2
WGK Germany3
FLUKA BRAND F CODES21
TSCAYes
HS Code29163900
Hazard Class8
Packing GroupII

AKOS BBS-00003909 - Upstream Downstream Industry

Raw MaterialsPhenylacetic acid
Phenylacetic acid
Chlorine

AKOS BBS-00003909 - Reference Information

NIST chemical information Information provided by: webbook.nist.gov (external link)
EPA chemical information Information provided by: ofmpub.epa.gov (external link)
use phenylacetyl chloride is an intermediate of fungicide benzoate and rodenticide bromine.
Used for perfume preparation and organic synthesis
Used as an intermediate in medicine, pesticide and perfume
This product is an intermediate in perfume and other organic synthesis.
Organic synthesis. Acylating agent.
Production method It is prepared by the reaction of phenylacetic acid and thionyl chloride. Mix equimolar phenylacetic acid and thionyl chloride, and react at room temperature to release sulfur dioxide and hydrogen chloride gas. When there is no longer a large amount of gas released, heat the reaction mixture to 30-40 ℃, keep the temperature for 25h, and add benzene with 1/4 volume of the mixture. The volatile matter is removed by low-temperature distillation, and the volatile matter is gradually reduced to 0.133kPa. After all volatile matter is removed, the 55-57 ℃(0.133kPa) fraction, namely phenylacetyl chloride, is evaporated. Yield 80-85%.
The preparation method is to add phenylacetic acid and thionyl chloride in the reaction kettle, heat and reflux for several hours, heat and decompress to remove the remaining thionyl chloride to obtain crude product, and distill the finished product under reduced pressure.
Last Update：2024-04-09 02:00:05
AKOS BBS-00003909
Supplier List
JIANGSU BSECHEM CHEMICAL TECHNOLOGY CO., LTD.
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Product Name: Phenylacetyl chloride Request for quotation
CAS: 103-80-0
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Nantong Reform Petro-Chemical CO., LTD.
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JIANGSU BSECHEM CHEMICAL TECHNOLOGY CO., LTD.
Spot supply
Product Name: Phenylacetyl chloride Request for quotation
CAS: 103-80-0
Tel: +86-17551318830
Email: r@reformchem.com
Mobile: +86-17551318830
QQ: 3787852685 Click to send a QQ messageSend QQ message
Nantong Reform Petro-Chemical CO., LTD.
Spot supply
Product Name: Phenylacetyl chloride Request for quotation
CAS: 103-80-0
Tel: +86-17551318830
Email: r@reformchem.com­
Mobile: +86-17551318830
QQ: 3785839865 Click to send a QQ messageSend QQ message
Jiangsu Pules Biotechnology Co.,Ltd.
Product Name: Phenylacetyl chloride Request for quotation
CAS: 103-80-0
Tel: 17505222756
Email: pules.cn@gmail.com
Mobile: +86-17551318830
Wechat: 17505222756
Hefei TNJ Chemical Industry Co.,Ltd.
Product Name: Phenylacetyl chloride Request for quotation
CAS: 103-80-0
Tel: 0086-551-65418684
Email: sales@tnjchem.com
　　　　 info@tnjchem.com
Mobile: 0086 189 4982 3763
QQ: 2881500840 Click to send a QQ message
Wechat: 0086 189 4982 3763
WhatsApp: 0086 189 4982 3763
Product List: View Catalog
Zouping Mingxing Chemical Co., Ltd.
Product Name: Phenylacetyl chloride Request for quotation
CAS: 103-80-0
Tel: 0086-13605431940
Email: xuli678323@126.com
Mobile: +86-13605431940
QQ: 56860987 Click to send a QQ message
Wechat: 13605431940
WhatsApp: 13605431940
Shanghai Yudiao Chemistry Technology Co.,Ltd
Product Name: Phenyl acetyl chloride Request for quotation
CAS: 103-80-0
Tel: +86 021-37285211
Email: info@yudiaochem.com
Mobile: +86 18964703211
QQ: 122752498 Click to send a QQ message
Wechat: yudiaochem
View History
AKOS BBS-00003909
Raw Materials for AKOS BBS-00003909
Phenylacetic acid
Phenylacetic acid
Chlorine
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