BENZILIC ACID HYDRAZIDE
BENZILIC HYDRAZIDE
CAS: 13050-38-9
Molecular Formula: C14H14N2O2
BENZILIC ACID HYDRAZIDE - Names and Identifiers
| Name | BENZILIC HYDRAZIDE |
| Synonyms | AKOS B014999 ASISCHEM Z67643 BENZILIC HYDRAZIDE ART-CHEM-BB B014999 TIMTEC-BB SBB009368 BENZILIC ACID HYDRAZIDE 2-HYDROXY-2,2-DIPHENYLETHANOHYDRAZIDE alpha-hydroxy-alpha-phenyl-benzeneaceticacihydrazide |
| CAS | 13050-38-9 |
| InChI | InChI=1/C14H14N2O2/c15-16-13(17)14(18,11-7-3-1-4-8-11)12-9-5-2-6-10-12/h1-10,18H,15H2,(H,16,17) |
BENZILIC ACID HYDRAZIDE - Physico-chemical Properties
| Molecular Formula | C14H14N2O2 |
| Molar Mass | 242.27 |
| Density | 1.253g/cm3 |
| Boling Point | 511.6°C at 760 mmHg |
| Flash Point | 263.2°C |
| Vapor Presure | 2.74E-11mmHg at 25°C |
| Storage Condition | Room Temprature |
| Refractive Index | 1.626 |
BENZILIC ACID HYDRAZIDE - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Hazard Class | IRRITANT |
BENZILIC ACID HYDRAZIDE - Introduction
2-Hydroxy-2, 2-diphenylacetohydrazide is an organic compound with the chemical formula C14H14N2O. The following is a description of its nature, use, preparation and safety information:
1. nature:
-Appearance: Colorless crystalline solid.
-Melting point: about 140-142°C.
-Solubility: Soluble in organic solvents such as ether, alcohol and chloroform, slightly soluble in water.
-Stability: relatively stable under normal storage and use conditions.
2. use:
-Chemical synthesis: As a reducing agent in organic synthesis, it is commonly used to reduce ketones, aldehydes and other compounds containing carbene and other functional groups.
-Drug synthesis: used as an intermediate or key raw material for the preparation of certain drugs. For example, it can be used in the synthesis of certain anti-cancer drugs.
-Electrochemistry: It is also used in the field of electrochemistry, and can act as an electron transfer agent in electrochemical synthesis and electrolytic reduction reactions.
3. Preparation method:
2-Hydroxy-2, 2-diphenylacetohydrazide can be synthesized by the following steps:
-The first step: benzaldehyde reacts with amines to generate imine. (e. g., reaction of benzaldehyde and aniline)
-The second step: The carbonyl group of the imine reacts with sodium hydroxide (NaOH) to form an amine oxime.
-The third step: the amine oxime is reduced by a reducing agent (such as sulfoxide) to obtain 2-hydroxy-2, 2-diphenylacetohydrazide.
4. Safety Information:
-2-Hydroxy-2, 2-diphenylacetohydrazide should be carefully protected from swallowing, inhalation, or contact with eyes and skin.
-Wear appropriate personal protective equipment such as lab gloves, goggles and protective clothing during use.
-in the handling or use of the process to strictly comply with the laboratory safety procedures.
-If you are unintentionally exposed or unwell, you should immediately seek medical advice and help.
-When storing, keep 2-hydroxy-2, 2-diphenylacetohydrazide in a dry, cool place, avoiding fire and oxidizing agents.
-Personnel engaged in related work should have relevant chemical knowledge and safety awareness.
1. nature:
-Appearance: Colorless crystalline solid.
-Melting point: about 140-142°C.
-Solubility: Soluble in organic solvents such as ether, alcohol and chloroform, slightly soluble in water.
-Stability: relatively stable under normal storage and use conditions.
2. use:
-Chemical synthesis: As a reducing agent in organic synthesis, it is commonly used to reduce ketones, aldehydes and other compounds containing carbene and other functional groups.
-Drug synthesis: used as an intermediate or key raw material for the preparation of certain drugs. For example, it can be used in the synthesis of certain anti-cancer drugs.
-Electrochemistry: It is also used in the field of electrochemistry, and can act as an electron transfer agent in electrochemical synthesis and electrolytic reduction reactions.
3. Preparation method:
2-Hydroxy-2, 2-diphenylacetohydrazide can be synthesized by the following steps:
-The first step: benzaldehyde reacts with amines to generate imine. (e. g., reaction of benzaldehyde and aniline)
-The second step: The carbonyl group of the imine reacts with sodium hydroxide (NaOH) to form an amine oxime.
-The third step: the amine oxime is reduced by a reducing agent (such as sulfoxide) to obtain 2-hydroxy-2, 2-diphenylacetohydrazide.
4. Safety Information:
-2-Hydroxy-2, 2-diphenylacetohydrazide should be carefully protected from swallowing, inhalation, or contact with eyes and skin.
-Wear appropriate personal protective equipment such as lab gloves, goggles and protective clothing during use.
-in the handling or use of the process to strictly comply with the laboratory safety procedures.
-If you are unintentionally exposed or unwell, you should immediately seek medical advice and help.
-When storing, keep 2-hydroxy-2, 2-diphenylacetohydrazide in a dry, cool place, avoiding fire and oxidizing agents.
-Personnel engaged in related work should have relevant chemical knowledge and safety awareness.
Last Update：2024-04-09 15:17:51
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CAS: 13050-38-9
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QQ: 3008007409
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CAS: 13050-38-9
Tel: 18301782025
Email: 3008007409@qq.com
Mobile: 18021002903
QQ: 3008007409
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