Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)-
[1-chloro-2-cyano-2-(4-chlorophenyl)hexane]
CAS: 98595-02-9
Molecular Formula: C13H15Cl2N
Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)- - Names and Identifiers
Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)- - Physico-chemical Properties
| Molecular Formula | C13H15Cl2N |
| Molar Mass | 256.17 |
| Density | 1.152±0.06 g/cm3(Predicted) |
| Boling Point | 365.1±27.0 °C(Predicted) |
| Physical and Chemical Properties | Chemical properties 1-chloro -2-cyano -2-(4-chlorophenyl) hexane pure product is a colorless transparent liquid, m.p.10 ℃, soluble in organic solvents such as acetone, toluene, xylene, etc., insoluble in water. |
| Use | Uses the production of bactericides myclobutanazole and mycophenolate previously used 1-bromo-2-cyano-2-(4-chlorophenyl) hexane as an intermediate, 1-chloro-2-cyano-2-(4-chlorophenyl) hexane has been used as an intermediate, which can reduce the cost of raw materials. |
Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)- - Upstream Downstream Industry
| Raw Materials | 2-(4-CHLOROPHENYL)-HEXANENITRILE |
Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)- - Nature
| EPA chemical information | Benzeneacetonitrile, .alpha.-butyl-4-chloro-.alpha.-(chloromethyl)- (98595-02-9) |
Last Update：2024-04-10 22:29:15
Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)- - Reference Information
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| Use | The production of fungicides mytinidazole and mibazole used 1-bromo-2-cyano-2-(4-chlorophenyl) hexane as an intermediate, and now 1-chloro-2-cyano-2-(4-chlorophenyl) hexane is used as an intermediate, which can reduce the cost of production raw materials. |
| production method | the preparation method is to add 2-(4-chlorophenyl) hexonitrile, NaOH aqueous solution and catalyst into the reaction kettle, slowly add slightly excess dichloromethane at a certain temperature, and then stir and react at this temperature for 3-4 hours. After the reaction, let it stand and stratify, divide the alkali aqueous solution, wash the organic layer with water, and then distill and recover dichloromethane and dehydrate. The residue is the product, and the product can also be purified by vacuum distillation. |
Last Update：2024-04-10 22:29:15
Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)- - Production method
the preparation method is to add 2-(4-chlorophenyl) hexanonitrile, NaOH aqueous solution and catalyst in the reaction kettle, slowly add a slightly excessive amount of dichloromethane at a certain temperature, and then stir the reaction at the temperature for 3~4 hours after adding dichloromethane. After the reaction, let it stand and stratify, divide the alkali aqueous solution, wash the organic layer with water, and then distill and recover dichloromethane and dehydrate. The residue is the product, and the product can also be purified by vacuum distillation.
Last Update：2024-04-10 22:29:15
Supplier List
View History
Raw Materials for Benzeneacetonitrile, α-butyl-4-chloro-α-(chloromethyl)-