Bis(2,2,2-trichloroethyl) azodicarboxyle

Bis(2,2,2-trichloroethyl) azodicarboxyle - Names and Identifiers

Name	bis(2,2,2-trichloroethyl) (E)-diazene-1,2-dicarboxylate
Synonyms	Bis(2,2,2-trichloroethyl) azodicarboxyle BIS(2,2,2-TRICHLOROETHYL) AZODICARBOXYLATE BEAZ Bis(2,2,2-trichloroethyl) azodicarboxylate AZODICARBOXYLIC ACID BIS(2,2,2-TRICHLOROETHYL) ESTER bis(2,2,2-trichloroethyl) (E)-diazene-1,2-dicarboxylate 1,2-Diazenedicarboxylic acid, 1,2-bis(2,2,2-trichloroethyl) ester
CAS	38857-88-4
InChI	InChI=1/C6H4Cl6N2O4/c7-5(8,9)1-17-3(15)13-14-4(16)18-2-6(10,11)12/h1-2H2/b14-13+

Bis(2,2,2-trichloroethyl) azodicarboxyle - Physico-chemical Properties

Molecular Formula	C6H4Cl6N2O4
Molar Mass	380.83
Density	1.78±0.1 g/cm3(Predicted)
Melting Point	109-111 °C (lit.)
Boling Point	380.7±42.0 °C(Predicted)
Flash Point	184.1°C
Vapor Presure	5.34E-06mmHg at 25°C
BRN	2141527
Storage Condition	2-8°C
Refractive Index	1.566

Bis(2,2,2-trichloroethyl) azodicarboxyle - Risk and Safety

Hazard Symbols	Xi - Irritant
Risk Codes	36/37/38 - Irritating to eyes, respiratory system and skin.
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing.
WGK Germany	3

Bis(2,2,2-trichloroethyl) azodicarboxyle - Introduction

bis(2,2,2-trichloroethyl) (E)-diazene-1,2-dicarboxylate is an organic compound with the chemical formula C8H8Cl6N2O4. It is a colorless crystalline solid with a strong odor. The following is a detailed description of its nature, use, formulation and safety information:

Nature:
-Appearance: Colorless crystalline solid
-Solubility: slightly soluble in water, soluble in organic solvents such as ether, alcohol and ketone
-Melting point: approx. 58-60°C
-Molecular weight: 281.88g/mol
-Density: 1.7g/cm³

Use:
bis(2,2,2-trichloroethyl) (E)-diazene-1,2-dicarboxylate is mainly used as a coupling agent and cross-linking agent in organic synthesis reactions. It can be used to synthesize polymer materials, plastics, rubber and coatings and other compounds. Due to its strong odor and toxicity, safety precautions are required when using it.

Preparation Method:
bis(2,2,2-trichloroethyl) (E)-diazene-1,2-dicarboxylate can be prepared by the following steps:
1. Reaction: 2,2, 2-trichloroethylamine and dicarboxylic acid (such as resorcinol dicarboxylic acid) react to generate the corresponding azodicarboxylic acid ester under alkaline conditions.
2. Crystallization: The desired colorless crystalline solid was obtained by crystallization.

Safety Information:
- bis(2,2,2-trichloroethyl) (E)-diazene-1,2-dicarboxylate has certain toxicity to the human body and may affect the central nervous system and respiratory system. Use with care to avoid inhalation, swallowing or skin contact.
-Use with appropriate precautions, such as gloves and goggles, and ensure that the operation is carried out in a well-ventilated laboratory.
-When disposing of waste, it is necessary to strictly comply with relevant laws and regulations to ensure the safety of the environment and human health.

Last Update：2024-04-10 22:29:15