Cyclohexanol, 1-allyl-
1-Allylcyclohexanol
CAS: 1123-34-8
Molecular Formula: C9H16O
Cyclohexanol, 1-allyl- - Names and Identifiers
Cyclohexanol, 1-allyl- - Physico-chemical Properties
| Molecular Formula | C9H16O |
| Molar Mass | 140.22 |
| Density | 0.9341 |
| Boling Point | 190°C (estimate) |
| pKa | 15.17±0.20(Predicted) |
| Storage Condition | -196°C |
| Refractive Index | 1.4756 |
| MDL | MFCD00021403 |
Cyclohexanol, 1-allyl- - Risk and Safety
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. |
Cyclohexanol, 1-allyl- - Reference Information
| production method | 1. preparation method: THF2mL, 1mmol of zinc powder are added to a reaction bottle filled with a dropping funnel, a solution of 1mmol of allyl bromide dissolved in 1mLTHF is slowly added in magnetic stirring reaction, and the reaction is carried out at room temperature for 30min. Slowly add cyclohexanone (2)1mmol dissolved in 1mLTHF solution, after adding continue stirring reaction, until the reaction is complete (TLC detection). Add a few drops of water and extract with ether. The ether extract is washed with saturated salt water and dried with anhydrous sodium sulfate. Concentrate to get a crude product. The crude product was purified by silica gel column to obtain compound ① (1) with 92% yield. Note: ① The following compounds can be synthesized by this method (Table I-5-11). [1] |
Last Update：2024-04-09 20:48:19
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