Molecular Formula | C14H14O4S2Zn |
Molar Mass | 375.77856 |
Melting Point | 251 °C (decomp)(Solv: ethanol (64-17-5)) |
CN201910837261.1
application date:
2019-09-05
Public/Announcement Number:
CN110642760A
Public/announcement date:
2020.01.03
applicant (patent):
Zhejiang jieshangjie New Materials Co., Ltd.
inventor:
National and provincial code:
CN330482
Abstract:
The invention discloses a synthesis method of zinc p-toluenesulfinate, comprising the following steps: S1, with p-Toluenesulfonyl chloride as the starting material, sodium sulfite as the reducing agent, water as the solvent, in the presence of an inorganic base, P-Toluenesulfonyl chloride is reduced to p-toluenesulfinate to obtain p-toluenesulfinate aqueous solution; S2, to the p-toluenesulfinate aqueous solution obtained in step S1, zinc chloride aqueous solution is added for reaction, the target product is obtained by filtering, washing with water and drying; The reaction temperature in step S2 is 72~88 ℃, and the reaction time is 60~120min; Preferably, the reaction temperature in step S2 is 79-83 ° C., and the reaction time is 80-100min. The synthetic method of the invention is safe and environment-friendly, has high yield, simple operation, convenient and easily available raw materials and low price, and is a synthetic route suitable for industrial production.
CN201921444951.2
application date:
2019-09-02
Public/Announcement Number:
CN211204755U
Public/announcement date:
2020.08.07
applicant (patent):
Jiaxing Jinli Chemical Co., Ltd.
inventor:
Zhu Jianhua , Li Yunxiao , Sun radium , Guo Jiajia , Jiang Shengmin
National and provincial code:
CN330402
Abstract:
The utility model discloses a flash dryer for drying zinc p-toluenesulfonate, which belongs to the technical field of dryer equipment, and comprises a bracket, a tank body and a feed pipe, and a bracket is installed on the surface of the tank body, the top of the surface of one side wall of the tank body is embedded with a feeding pipe, both sides of the bottom surface of the tank body are equipped with a driving motor, the inner cavity of the tank body is equipped with a stirring paddle, and the stirring paddle is connected to the input end of the driving motor through a rotating shaft. The utility model can form a powerful rotating wind field in the tank body through multiple groups of driving motors and stirring blades, and the hot air is injected into the tank body, so that the material can be dried and dehydrated, in addition, the dehydrated material can be discharged with the rise of the hot air flow. Through the anti-adhesive coating and the thermal insulation cotton, the material can be prevented from sticking to the inner wall surface of the tank body, and the heat preservation effect can be achieved, at the same time through the sewage pipe, and can be discharged after cleaning the sewage, improve the service life of the flash dryer.
202023188001
applicant (patent):
Jiaxing Jinli Chemical Co., Ltd.
inventor:
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