Glycine,N-(2-iodobenzoyl)-
2'-IODOHIPPURIC ACID
CAS: 147-58-0
Molecular Formula: C9H8INO3
Glycine,N-(2-iodobenzoyl)- - Names and Identifiers
| Name | 2'-IODOHIPPURIC ACID |
| Synonyms | O-IODOHIPPURIC ACID 2-IODOHIPPURIC ACID 2'-IODOHIPPURIC ACID (2-IODOBENZOYL)GLYCINE N-(2-IODOBENZOYL)GLYCINE Glycine,N-(2-iodobenzoyl)- o-Iodohippuric Acid (100 mg) o-Iodohippuric acid for synthesis |
| CAS | 147-58-0 |
| EINECS | 205-693-5 |
Glycine,N-(2-iodobenzoyl)- - Physico-chemical Properties
| Molecular Formula | C9H8INO3 |
| Molar Mass | 305.07 |
| Melting Point | 170-172 °C (lit.) |
| Appearance | Form Solid, color White to Off-White |
| Storage Condition | Store below +30°C. |
| MDL | MFCD00002694 |
| Use | Overview 2-iodohippuric acid is also called o-iodohippuric acid, N-2-iodobenzoyl glycine, which can be prepared by the acylation of glycine and iodobenzoyl chloride. |
Glycine,N-(2-iodobenzoyl)- - Risk and Safety
| Safety Description | S22 - Do not breathe dust. S24/25 - Avoid contact with skin and eyes. |
| WGK Germany | 3 |
| HS Code | 2924 29 70 |
Glycine,N-(2-iodobenzoyl)- - Upstream Downstream Industry
Glycine,N-(2-iodobenzoyl)- - Nature
| Solubility | DMSO (Slightly), Methanol (Slightly) |
| BRN | 1877943 |
Last Update：2024-04-10 22:29:15
Glycine,N-(2-iodobenzoyl)- - Preparation
General/Typical Procedure: Preparation of N-2-bromobenzoylglycine: Dissolve glycine (0.948g,12.628mmol) in water (50mL), and then dissolve in 2-bromobenzoyl chloride (0.649g,2.957mmol) in aqueous solution. NaOH solution (0.380g,9.500mmol) was added to the solution simultaneously in batches to keep the pH of the mixture slightly alkaline. After adding the parts, stir the mixture vigorously. Crushed ice is added to the solution, and then concentrated HCl is added drop by drop until the mixture is acidified (pH2-3). The mixture was then cooled in a refrigerator, then filtered, washed the precipitate several times with water to remove excess glycine, and then dried under vacuum to give N-2-bromobenzoylglycine, a white crystalline solid (yield 0.565g,74%). Preparation of N-2-iodobenzoyl glycine: As described in N-2-bromobenzoyl glycine, glycine (2.431g,32.383mmol), iodobenzoyl chloride (2.157g,8.950mmol) and NaOH(0.712g,17.800mmol) were reacted to obtain N-2-iodobenzoyl glycine, a white crystalline solid (yield 1.531g,62%).
Last Update：2024-04-10 22:29:15
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Raw Materials for Glycine,N-(2-iodobenzoyl)-