Iron bis(acetylacetonate)
bis(pentane-2,4-dionato-O,O')iron
CAS: 14024-17-0
Molecular Formula: C10H14FeO4
Iron bis(acetylacetonate) - Names and Identifiers
| Name | bis(pentane-2,4-dionato-O,O')iron |
| Synonyms | AI3-61033 Ferroacetylacetonate (Acetylacetonato)iron Bis(acetylacetonato)iron Iron bis(acetylacetonate) (Acetylacetonato)iron (ii) Bis(2,4-pentanedionato)iron bis(1,4-Pentanedionato) iron Bis(pentane-2,4-dionato-O,O')iron bis(2,4-pentanedionato-O,O')-Iron bis(pentane-2,4-dionato-O,O')iron Iron, bis(2,4-pentanedionato-O,O')- iron(2+) bis[(2Z)-4-oxopent-2-en-2-olate] |
| CAS | 14024-17-0 |
| EINECS | 237-851-4 |
| InChI | InChI=1/2C5H8O2.Fe/c2*1-4(6)3-5(2)7;/h2*3,6H,1-2H3;/q;;+2/p-2/b2*4-3- |
Iron bis(acetylacetonate) - Physico-chemical Properties
| Molecular Formula | C10H14FeO4 |
| Molar Mass | 254.06 |
| Melting Point | 175°C (dec.)(lit.) |
| Boling Point | 187.6°C at 760 mmHg |
| Flash Point | 71.9°C |
| Vapor Presure | 0.174mmHg at 25°C |
| Appearance | Dark brown powder |
| Storage Condition | Inert atmosphere,Room Temperature |
| Sensitive | Easy to absorb moisture and sensitive to air |
| MDL | MFCD00144506 |
Iron bis(acetylacetonate) - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
Iron bis(acetylacetonate) - Reference Information
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| traits | dark brown powder |
| use | organic synthesis catalyst. |
| production method | 25g FeCl2 · 4H2O is dissolved in 50mL of degassing water containing a small amount of sodium dithionite in order to reduce a small amount of ferric iron impurities. This solution was added to a 300mL aqueous solution containing 27.3mL of hexahydropyridine and 28.1mL of acetylacetone. After 15min, the precipitate generated was filtered and washed with water, ethanol and ether in turn. The brownish-yellow substance was transferred to a vacuum dryer and dried at 0.133Pa for 6h. Then the yellow powder of Fe(acac)2 · 2H2O was heated to 90°C at a pressure of 0.133Pa and kept for at least 12h to remove the crystal water. The yellow-brown crystal obtained is Fe(acac)2. |
Last Update：2024-04-10 22:29:15
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