Name | dibenzoyl disulphide |
Synonyms | Disulfide,dibenzoyl dibenzoyl disulphide Dibenzoyl persulfide Benzoic dithioperoxyanhydride benzenecarbothioic acid S-(benzoylthio) ester |
CAS | 644-32-6 |
EINECS | 211-413-2 |
InChI | 1/C14H10o2S2/C15-13(11-7-3-1-4-8-11)17-18-14(16)12-9-5-2-6-10-12/H1-10 |
Molecular Formula | C14H10O2S2 |
Molar Mass | 274.36 |
Density | 1.3504 (rough estimate) |
Melting Point | 134.5°C |
Boling Point | 387.34°C (rough estimate) |
Refractive Index | 1.5341 (estimate) |
Physical and Chemical Properties | Chemical properties prismatic or flaky crystals. Melting point 133 ℃. Soluble in ether, chloroform, petroleum ether. |
Use | Uses Organic synthesis intermediates. |
Downstream Products | Dibenzoic thioanhydride |
First pass hydrogen sulfide into potassium hydroxide ethanol solution to saturation, stir and cool to 10-15 ℃, and add benzoyl chloride dropwise. Filter out the potassium chloride precipitated by the reaction, slowly add solid iodine, and keep it at 10-15 ℃. During the iodization process, dibenzoyl disulfide precipitates out.