3,4-二咖啡酰奎宁酸
3,4-二咖啡酰奎宁酸((1S,3R,4R,5R)-3,4-Bis[[(E)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy]-1,5-dihydroxycyclohexane-1-carboxylic acid)
CAS: 14534-61-3
化学式: C25H24O12
| 中文名 | 3,4-二咖啡酰奎宁酸 |
| 英文名 | (1S,3R,4R,5R)-3,4-Bis[[(E)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy]-1,5-dihydroxycyclohexane-1-carboxylic acid |
| 别名 | 异绿原酸B 异绿原酸B(3 二咖啡酰奎宁酸 3,4-二咖啡酰奎宁酸 异绿原酸B(3,4-二咖啡酰奎宁酸) 3,4-二咖啡酰奎宁酸(异绿原酸 B) ISOCHLOROGENIC ACID B 异绿原酸B ISOCHLOROGENIC ACID B 异绿原酸B 标准品 |
| 英文别名 | Isochlorogenic acid B ISOCHLOROGENIC ACID B(RG) 3,4-Dicaffeoylquinic acid Isochlorogenic acid B, froM Lonicera japonica Isochlorogenic acid B,3,4-Dicaffeoylquinic acid 1β,3β-Dihydroxy-4β,5α-bis[[3-(3,4-dihydroxyphenyl)-1-oxo-2-propenyl]oxy]-1α-cyclohexanecarboxylic acid (1S)-4β,5α-Bis[[3-(3,4-dihydroxyphenyl)-1-oxo-2-propenyl]oxy]-1β,3β-dihydroxycyclohexanecarboxylic acid (1R,4R,5R)-3,4-bis{[(2E)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy}-1,5-dihydroxycyclohexanecarboxylic acid (1S)-1α,5α-Dihydroxy-3β,4α-bis[[3-(3,4-dihydroxyphenyl)-1-oxo-2-propenyl]oxy]-1β-cyclohexanecarboxylic acid (1S,3R,4R,5R)-3,4-bis{[(2E)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy}-1,5-dihydroxycyclohexanecarboxylic acid (1S,3R,4R,5R)-3,4-Bis[[(E)-3-(3,4-dihydroxyphenyl)prop-2-enoyl]oxy]-1,5-dihydroxycyclohexane-1-carboxylic acid |
| CAS | 14534-61-3 |
| 化学式 | C25H24O12 |
| 分子量 | 516.45 |
| InChI | InChI=1/C25H24O12/c26-15-5-1-13(9-17(15)28)3-7-21(31)36-20-12-25(35,24(33)34)11-19(30)23(20)37-22(32)8-4-14-2-6-16(27)18(29)10-14/h1-10,19-20,23,26-30,35H,11-12H2,(H,33,34)/b7-3+,8-4+/t19-,20?,23-,25-/m1/s1 |
| 密度 | 1?+-.0.1 g/cm3(Predicted) |
| 熔点 | >117°C (sub.) |
| 沸点 | 810.8±65.0 °C(Predicted) |
| 比旋光度 | -225 (MeOH) |
| 闪点 | 274.9°C |
| 蒸汽压 | 8.9E-28mmHg at 25°C |
| 溶解度 | 甲醇 (微溶) |
| 折射率 | 1.719 |
| 酸度系数 | 3.70±0.50(Predicted) |
| 存储条件 | Sealed in dry,Store in freezer, under -20°C |
| 外观 | 固体 |
| 颜色 | Off-White to Light Yellow |
| 物化性质 | 类色结晶粉末，可溶于甲醇、乙醇、DMSO等有机溶剂，来源于金银花，忍冬，杜仲。 |
| MDL号 | MFCD22375481 |
| 体外研究 | 3,4-Dicaffeoylquinic acid acts as a greater primary antioxidant than its methanol extract, by having higher ferric reducing activity (EC 50 2.18 μg/ml), β-carotene bleaching activity (EC 50 23.85 μg/ml) and DPPH scavenging activity (EC 50 68.91 μg/ml). 3,4-Dicaffeoylquinic acid exhibits a remarkable dose-dependent inhibitory effect on NCI-H23 (human lung adenocarcinoma) cell lines (EC 50 3.26 μg/ml) and is found to be apoptotic in nature based on a clear indication of DNA fragmentation. 3,4-Dicaffeoylquinic acid also displays a concentration-dependent α-glucosidase inhibition with EC 50 241.80 μg/ml. |
| 安全术语 | 24/25 - 避免与皮肤和眼睛接触。 |
| WGK Germany | 3 |
| 海关编号 | 29189900 |
| 参考资料 展开查看 | 1. 张莉 周娟娟. UPLC法同时测定银翘解毒合剂中10种成分[J]. 中成药 2018 40(08):86-89. 2. 李小军 张姝砣 穆云妹 等. "一测多评"法测定平卧菊三七中绿原酸类成分[J]. 中国医院药学杂志 2015(22):2007-2011. 3. 王俊俊 张俐 郭青 等. 一测多评法测定8个银翘解毒系列制剂中的7种酚酸类成分的含量[J]. 药学学报 2015 050(004):480-485. 4. 高利利 倪健 于颖超 等. 双黄连颗粒HPLC指纹图谱及化学模式识别分析[J]. 中国中医药信息杂志 2019 026(010):60-65. 5. 董婷, 周建良, 赵维良,等. 基于指纹图谱的银翘解毒颗粒质量评价[J]. 中国现代应用药学, 2018, 35(09):68-72. 6. 刘鑫, 牛子冉, 梅丹,等. 异绿原酸B对肝损伤小鼠的保护作用及其机制[J]. 医药导报 2020年39卷7期, 895-899页, ISTIC PKU CA, 2020. 7. 王玲娜, 刘红燕, 李佳,等. 忍冬叶有效成分含量与气候因子的灰色关联分析[J]. 山东农业科学, 2014(11):57-60. 8. 马云, 王尧尧, 王蕾,等. 忍冬花发育期间形态与13种活性成分含量变化[J]. 中药材, 2018, 041(007):1559-1565. 9. 王春驰, 周婷婷, 纪圣君,等. 返魂草药材提取方法考察与特征图谱建立[J]. 长春中医药大学学报, 2019, 035(002):322-325. 10. 王玲娜,苏征,刘星劼,张芳,刘谦,张永清.金银花活性成分与生态因子相关性研究[J].中国实验方剂学杂志,2016,22(17):27-31. 11. 刘宗洋,昝珂,沙拉麦提·艾力,吴霞,过立农,马双成,郑健,陈筱清.维药驱虫斑鸠菊HPLC-ELSD特征图谱和2个主要成分含量测定[J].药物分析杂志,2020,40(09):1702-1708. 12. 王玲娜, 孙希芳, 张芳,等. 不同发育时期金银花颜色与活性成分的相关性分析[J]. 中草药, 2017, 15(v.48;No.602):171-177. 13. 陈冰冰, 汤晟凌, 吕伟旗. 土圞儿中3种成分含量的变异规律[J]. 中成药, 2016(12):2636-2640. 14. 王玲娜 刘红燕 张金 等. "一测多评法"与外标法测定金银花中8种活性成分含量[J]. 中国实验方剂学杂志 2014 20(20):57-61. 15. 苏征 王玲娜 张芳 等. 不同产地忍冬藤HPLC指纹图谱比较研究[J]. 时珍国医国药 2017(05):193-195. 16. 黄玉娟, 舒一崧, 孔静, et al. 基于特征图谱的金银花与山银花(灰毡毛忍冬)质量表征比较研究[J]. 环球中医药 2020年13卷4期, 600-610页, ISTIC CA, 2020. 17. 路俊仙, 吕凌, 张才波. 忍冬4个药用部位中11种化学成分的含量测定[J]. 中药材, 2019(5). 18. 路俊仙, 吕凌, 张才波. 金银花和灰毡毛忍冬多成分定性的指纹图谱比较[J]. 中华中医药杂志, 2019, 034(007):3215-3219. 19. 王玲娜,张芳,李佳,刘红燕,姜秋,张永清.金银花新品种“华金6号”药材品质比较研究[J].中药材,2019,42(09):2030-2035. 20. 谭春梅,黄琴伟,王征南,马临科,赵维良.复方鱼腥草合剂特征图谱及基于Orbitrap超高分辨质谱结合多元数理统计方法的成分分析[J].药物分析杂志,2020,40(10):1770-1779. 21. 蔡芷辰,陈欢,杨蓉,陈佳佳,王程成,谈梦霞,陈佳丽,梅余琪,魏丽芳,殷圣鑫,刘训红.基于液相色谱-串联质谱结合多元统计分析盐胁迫下金银花代谢产物积累的变化[J].南京中医药大学学报,2020,36(05):584-592. 22. 李丽丽,李月,卢恒,王晓.基于液相色谱-质谱法的不同花期金银花代谢组学分析[J].分析测试学报,2020,39(12):1501-1507. 23. 胡飞凤,黄文康.高效液相色谱波长切换技术对复方野菊感冒颗粒中8种成分的含量测定[J].中国新药与临床杂志,2020,39(10):618-622. 24. Min Yang, Feng Zou, Qingxin Shi, Simin Ji, Xuanyuan Wang, Xingliang Xiang, Wan Li, Shuna Jin, Rongzeng Huang & Chengwu Song (2018) An efficient approach for enrichment of three isochlorogenic acids from Kuding tea using MCI-GEL resin, Journal of Liquid Chr 25. Chenxi Yang, Chenglin Song, Yitong Liu, Jiao Qu, Haibo Li, Wei Xiao, Lingdong Kong, Huiming Ge, Yang Sun, Wen Lv, Re-Du-Ning injection ameliorates LPS-induced lung injury through inhibiting neutrophil extracellular traps formation, Phytomedicine, Volume 90 26. Cai, Z, Liao, H, Wang, C, et al. A comprehensive study of the aerial parts of Lonicera japonica Thunb. based on metabolite profiling coupled with PLS-DA. Phytochemical Analysis. 2020; 31: 786– 800. https://doi.org/10.1002/pca.2943 27. Li, Moying, et al. "Method for rapidly discovering active components in Yupingfeng granules by UPLC‐ESI‐Q‐TOF‐MS." Journal of Mass Spectrometry 55.10 (2020): e4627.https://doi.org/10.1002/jms.4627 28. Xue, Gen, et al. "Integrating Study on Qualitative and Quantitative Characterization of the Major Constituents in Shuanghuanglian Injection with UHPLC/Q-Orbitrap-MS and UPLC-PDA." Journal of Analytical Methods in Chemistry 2021 (2021).https://doi.org/10.11 29. Hengqiang Zhao, Changjiangsheng Lai, Minmin Zhang, Siduo Zhou, Qian Liu, Daijie Wang, Yanling Geng, Xiao Wang,An improved 2D-HPLC-UF-ESI-TOF/MS approach for enrichment and comprehensive characterization of minor neuraminidase inhibitors from Flos Lonicera 30. Hengqiang Zhao, Changjiangsheng Lai, Minmin Zhang, Siduo Zhou, Qian Liu, Daijie Wang, Yanling Geng, Xiao Wang,An improved 2D-HPLC-UF-ESI-TOF/MS approach for enrichment and comprehensive characterization of minor neuraminidase inhibitors from Flos Lonicera 31. Hengqiang Zhao, Changjiangsheng Lai, Minmin Zhang, Siduo Zhou, Qian Liu, Daijie Wang, Yanling Geng, Xiao Wang,An improved 2D-HPLC-UF-ESI-TOF/MS approach for enrichment and comprehensive characterization of minor neuraminidase inhibitors from Flos Lonicera 32. Hengqiang Zhao, Changjiangsheng Lai, Minmin Zhang, Siduo Zhou, Qian Liu, Daijie Wang, Yanling Geng, Xiao Wang,An improved 2D-HPLC-UF-ESI-TOF/MS approach for enrichment and comprehensive characterization of minor neuraminidase inhibitors from Flos Lonicera 33. Zhengqi Pan, Qinfen Wu, Zhe Xie, Qiang Wu, Xinti Tan, Xin Wang,Upregulation of HSP72 attenuates tendon adhesion by regulating fibroblast proliferation and collagen production via blockade of the STAT3 signaling pathway,Cellular Signalling,Volume 71,2020,10 34. [IF=4.411] Ai-Li Guo et al."Influence of Sulfur Fumigation on the Chemical Constituents and Antioxidant Activity of Buds of Lonicera japonica."Molecules. 2014 Oct;19(10):16640-16655 35. 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3,4-二咖啡酰奎宁酸 - 简介
3,4-二咖啡酰奎宁酸（3,4-dicaffeoylquinic acid）是一种化学物质，属于多酚类化合物。下面是关于它的性质、用途、制法和安全信息的介绍：
性质：
- 外观：呈黄色结晶粉末
- 溶解性：在水中溶解度较低，易溶于乙醇和醚类溶剂
- 稳定性：在中性和弱酸性条件下相对稳定，但在强酸性和碱性条件下会分解
用途：
- 天然产物：3,4-二咖啡酰奎宁酸被发现广泛存在于多种植物中，如菊花、艾草、牡丹等。
- 药理作用：研究表明，3,4-二咖啡酰奎宁酸具有抗糖尿病、抗癌、抗心血管疾病等多种药理作用。它可以抑制炎症反应、减少氧化应激并保护细胞免受损害。
制法：
3,4-二咖啡酰奎宁酸可以通过提取自含有该化合物的植物材料，然后进行纯化和结晶得到。另外，也可以通过化学合成方法合成得到。
安全信息：
3,4-二咖啡酰奎宁酸是一种天然物质，相对较安全。但对于过敏体质的人群应谨慎使用，因为可能引起过敏反应。在使用时应遵循适当的剂量，避免长期大剂量使用。
性质：
- 外观：呈黄色结晶粉末
- 溶解性：在水中溶解度较低，易溶于乙醇和醚类溶剂
- 稳定性：在中性和弱酸性条件下相对稳定，但在强酸性和碱性条件下会分解
用途：
- 天然产物：3,4-二咖啡酰奎宁酸被发现广泛存在于多种植物中，如菊花、艾草、牡丹等。
- 药理作用：研究表明，3,4-二咖啡酰奎宁酸具有抗糖尿病、抗癌、抗心血管疾病等多种药理作用。它可以抑制炎症反应、减少氧化应激并保护细胞免受损害。
制法：
3,4-二咖啡酰奎宁酸可以通过提取自含有该化合物的植物材料，然后进行纯化和结晶得到。另外，也可以通过化学合成方法合成得到。
安全信息：
3,4-二咖啡酰奎宁酸是一种天然物质，相对较安全。但对于过敏体质的人群应谨慎使用，因为可能引起过敏反应。在使用时应遵循适当的剂量，避免长期大剂量使用。
最后更新：2024-04-09 20:52:54
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产品名: (1S,3R,4R,5R)-3,4-双(((E)-3-(3,4-二羟基苯基)丙烯酰)氧基)-1,5-二羟基环己烷甲酸 询盘CAS: 14534-61-3
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产品描述: (1S,3R,4R,5R)-3,4-双(((E)-3-(3,4-二羟基苯基)丙烯酰)氧基)-1,5-二羟基环己烷甲酸,98%,Amole/阿摩尔
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产品名: 3,4-Dicaffeoylquinic acid 去供应商网站查看 询盘CAS: 14534-61-3
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产品名: 3,4-二咖啡酰奎宁酸 去供应商网站查看 询盘CAS: 14534-61-3
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产品描述: Isochlorogenic acid B is a reference substance of a common phytochemical found i 更多
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产品名: 异绿原酸B(10mM in DMSO,无菌) 去供应商网站查看 询盘CAS: ID02401
产地: 北京
包装: 1ml/瓶
规格: ID02401-1ml
价格: 电话、微信、QQ、邮件
库存: 现询
电话: 010-50973130
手机: 18101056239(微信同号)
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产品描述: 产品覆盖：小分子化合物、分析对照品、染色试剂、生化试剂盒、细胞生物学、分子生物学、抗体、蛋白、多肽、ELISA试剂盒、微生物培养、化学合成、仪器耗材、CRO技术 更多
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产品名: (1S,3R,4R,5R)-3,4-双(((E)-3-(3,4-二羟基苯基)丙烯酰)氧基)-1,5-二羟基环己烷甲酸 询盘CAS: 14534-61-3
产地: 上海
包装: 100mg；10mg；1mg；25mg；50mg；5mg
规格: 98%
价格: 电话、微信、QQ、邮件
库存: 现货
电话: 400-968-2212
手机: 18916960931
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微信: 18916960931
产品描述: (1S,3R,4R,5R)-3,4-双(((E)-3-(3,4-二羟基苯基)丙烯酰)氧基)-1,5-二羟基环己烷甲酸,98%,Amole/阿摩尔
提供多种规格现货供应
产品名: 3,4-Dicaffeoylquinic acid 去供应商网站查看 询盘CAS: 14534-61-3
产地: 美国
包装: 10 mM * 1 mL;1 mg;5 mg;10 mg;25 mg;50 mg;100 mg
规格: HY-N0057
库存: 现货，货期：1-2天
电话: 021-38924433; 021-58955995
手机: 18019480960
电子邮件: sales@medchemexpress.cn
产品描述: 产品覆盖：8万多种抑制剂，11000+靶点蛋白，数百款试剂盒，200+生物活性化合物库，天然产物，抗体等. 纯度: 98.64%
现货供应
产品名: 3,4-二咖啡酰奎宁酸 去供应商网站查看 询盘CAS: 14534-61-3
产地: 其他
包装: 20 mg
价格: $279
库存: In stock
电话: +16314854226
手机: +16314854226
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产品描述: Isochlorogenic acid B is a reference substance of a common phytochemical found i 更多
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