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(S)-N-Boc-2-Hydroxymethylmorpholine

(S)-N-Boc-2-Hydroxymethylmorpholine

CAS: 135065-76-8

Molecular Formula: C10H19NO4

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(S)-N-Boc-2-Hydroxymethylmorpholine - Names and Identifiers

Name (S)-N-Boc-2-Hydroxymethylmorpholine
Synonyms (S)-N-Boc-2-HydroxyMethyl...
N-Boc-(S)-3-morpholine-methanol
(S)-N-Boc-2-Hydroxymethylmorpholine
(S)-N-BOC-2-HYDROXYMETHYLMORPHOLINE
(S)-4-BOC-2-HYDROXYMETHYL-MORPHOLINE
(S)-ter-butyl 2-(hydroxymethyl)morpholine-4-carboxylate
tert-butyl (2S)-2-(hydroxymethyl)morpholine-4-carboxylate
tert-Butyl (2S)-2-(hydroxyMethyl)Morpholine-4-carboxylate
(S)-2-Hydroxymethylmorpholine-4-carboxylic acid tert-butyl ester
(2S)-2-hydroxymethyl-morpholine-4-carboxylic acid tert-butyl ester
4-Morpholinecarboxylic acid, 2-(hydroxyMethyl)-, 1,1-diMethylethyl ester, (2S)-
CAS 135065-76-8
EINECS 696-348-1
InChI InChI=1/C10H19NO4/c1-10(2,3)15-9(13)11-4-5-14-8(6-11)7-12/h8,12H,4-7H2,1-3H3/t8-/m0/s1

(S)-N-Boc-2-Hydroxymethylmorpholine - Physico-chemical Properties

Molecular FormulaC10H19NO4
Molar Mass217.26
Density1.118
Melting Point60-62 °C
Boling Point321 °C
Flash Point148 °C
Water SolubilitySlightly soluble in water.
Vapor Presure2.53E-05mmHg at 25°C
AppearanceWhite solid
pKa14.36±0.10(Predicted)
Storage Conditionunder inert gas (nitrogen or Argon) at 2-8°C
SensitiveLight Sensitive
Refractive Index1.474
MDLMFCD09260606

(S)-N-Boc-2-Hydroxymethylmorpholine - Reference Information

use N-tert-butoxycarbonyl-(S)-2-morpholine methanol is a useful research chemical.
N-tert-butoxycarbonyl-(S)-2-morpholine methanol is mainly used in medicine and pesticide intermediates.
preparation at 0 ℃, borane (1M,20mL) was dropwise added to the solution of (S)-4-(tert-butoxycarbonyl) morpholine -2-formic acid (2.50g,10.8mmol) in THF(25mL)
, for 15min. After adding, warm the reaction mixture to room temperature and stir for 2 small
. At 0°C, the reaction mixture was quenched with MeOH/AcOH(9:1,10mL). The mixture was then concentrated and the residue poured into 35mL of water and 35mL
EtOAc. The organic layer was washed with a saturated Na2CO3(30mL) aqueous solution, dried with Na2SO4 and
concentrated to obtain N-tert-butoxycarbonyl-(S)-2-morpholine methanol (2.6g,100%), which was a colorless oil.
Last Update：2024-04-10 22:29:15
(S)-N-Boc-2-Hydroxymethylmorpholine
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View History
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