1-methylcyclohexanamine
N-Methylcyclohexylamine
CAS: 100-60-7
Molecular Formula: C7H15N
1-methylcyclohexanamine - Names and Identifiers
1-methylcyclohexanamine - Physico-chemical Properties
| Molecular Formula | C7H15N |
| Molar Mass | 113.2 |
| Density | 0.868 g/mL at 25 °C (lit.) |
| Melting Point | -9--7 °C (lit.) |
| Boling Point | 149 °C (lit.) |
| Flash Point | 85°F |
| Water Solubility | 5.4 g/100 mL (20 ºC) |
| Solubility | 54g/l |
| Vapor Presure | 11 mm Hg ( 40 °C) |
| Vapor Density | 4 (vs air) |
| Appearance | Liquid |
| Specific Gravity | 0.855 (20/4℃) |
| Color | Clear colorless to yellow |
| BRN | 1523664 |
| pKa | 11.03±0.20(Predicted) |
| PH | 12 (10g/l, H2O, 20℃) |
| Storage Condition | Keep in dark place,Inert atmosphere,Room temperature |
| Sensitive | Air Sensitive |
| Explosive Limit | 2.2-10.5%(V) |
| Refractive Index | n20/D 1.456(lit.) |
| Physical and Chemical Properties | Character: colorless transparent liquid. boiling point 147~151 ℃ relative density 0.868 refractive index 1.4456 flash point 29 ℃ solubility it is miscible with a variety of organic solvents and slightly soluble in water. |
| Use | Used as intermediates in pharmaceuticals and dyes |
1-methylcyclohexanamine - Risk and Safety
| Hazard Symbols | C - Corrosive |
| Risk Codes | R10 - Flammable R21/22 - Harmful in contact with skin and if swallowed. R35 - Causes severe burns R20/21/22 - Harmful by inhalation, in contact with skin and if swallowed. |
| Safety Description | S16 - Keep away from sources of ignition. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) |
| UN IDs | UN 2734 8/PG 2 |
| WGK Germany | 1 |
| RTECS | GX1529000 |
| TSCA | Yes |
| HS Code | 29213099 |
| Hazard Note | Corrosive |
| Hazard Class | 8 |
| Packing Group | II |
1-methylcyclohexanamine - Upstream Downstream Industry
| Downstream Products | bromohexine hydrochloride |
1-methylcyclohexanamine - Reference Information
| NIST chemical information | information provided by: webbook.nist.gov (external link) |
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| Use | used as intermediate of medicine and dye intermediate of medicine and dye. Used as an intermediate for the drug bromohexylamine hydrochloride. |
| production method | 1. Cyclohexylamine as raw material. Derived from the reaction of cyclohexanone with methylamine. The aluminum sheet was immersed in methanol, and then the high mercury chloride was added. The immersion was continued for 2H, and the temperature was not more than 55 ° C., and the soaking solution was removed. Ethanol was added to the above activated aluminum sheet, and a mixed solution of methylamine and cyclohexanone was added dropwise with stirring, and the mixture was heated to reflux and left overnight. 10% sodium hydroxide solution was added for alkalization, and the mixture was extracted twice with benzene, washed with water, and then distilled to recover benzene, and then N-methylcyclohexylamine was distilled off. The yield was about 80%. |
Last Update：2024-04-09 19:55:45
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Downstream Products for 1-methylcyclohexanamine