1009826-93-0
4-Pyrimidinecarboxylicacid, 5-bromo-, methyl ester
CAS: 1009826-93-0
Molecular Formula: C6H5BrN2O2
1009826-93-0 - Names and Identifiers
1009826-93-0 - Physico-chemical Properties
| Molecular Formula | C6H5BrN2O2 |
| Molar Mass | 217.02 |
| Density | 1.669±0.06 g/cm3(Predicted) |
| Boling Point | 279.7±20.0 °C(Predicted) |
| Flash Point | 123 °C |
| pKa | -2.35±0.16(Predicted) |
| Storage Condition | Sealed in dry,Room Temperature |
| Sensitive | Irritant |
| MDL | MFCD11111841 |
1009826-93-0 - Reference Information
| Introduction | Methyl 5-bromo-4-pyrimidinoformate is an organic intermediate that can be used as a raw material to prepare 5-bromopyrimidin-4-formyl chloride first, and then esterify with methanol to obtain. |
| use | methyl 5-bromo-4-pyrimidine formate is a carboxylate derivative and can be used as an intermediate in organic synthesis. |
| Preparation | 5-bromopyrimidine -4-carboxylic acid (prepared according to the method described in U.S. Patent 4,110,450)(1.0 equivalents, 6.14g,30.2mmol) is suspended in CH2Cl2(100ml). Oxalyl chloride (1.1 equivalent, 2.9ml, 33.0mmol) was added, followed by 2 drops of DMF. Stir the mixture overnight at room temperature and remove volatiles in vacuum. The residue was absorbed into MeOH(50ml) and heated. After evaporating MeOH in vacuum to , the compound is dissolved in CH2Cl2 and loaded on a pre-filled silica gel column. Use 20% ethyl acetate in hexane to elute the substance. The solvent was evaporated to obtain methyl 5-bromo-4-pyrimidinic formate, which is a light orange crystalline solid. |
Last Update：2024-04-09 15:16:37
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View History
1009826-93-0
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