117007-52-0
3-Iodo-7-aza-1H-azaindazole
CAS: 117007-52-0
Molecular Formula: C6H4IN3
117007-52-0 - Names and Identifiers
| Name | 3-Iodo-7-aza-1H-azaindazole |
| Synonyms | 3-Iodo- 3-Iodo-7-aza-1H-indazole 3-Iodo-7-aza-1H-azaindazole 3-Iodo-1H-pyrazolo[3,4-b]... 3-iodo-2H-pyrazolo[3,4-b]pyridine 3-iodo-1H-pyrazolo[3,4-b]pyridine 1H-Pyrazolo[3,4-b]pyridine, 3-iodo- |
| CAS | 117007-52-0 |
| InChI | InChI=1/C6H4IN3/c7-5-4-2-1-3-8-6(4)10-9-5/h1-3H,(H,8,9,10) |
117007-52-0 - Physico-chemical Properties
| Molecular Formula | C6H4IN3 |
| Molar Mass | 245.02 |
| Density | 2.219±0.06 g/cm3(Predicted) |
| Melting Point | 177-179°C |
| Boling Point | 379.8±22.0 °C(Predicted) |
| Solubility | Chloroform, DMSO |
| Appearance | Solid |
| Color | Pale Yellow |
| pKa | 7.96±0.40(Predicted) |
| Storage Condition | Keep in dark place,Inert atmosphere,2-8°C |
| Refractive Index | 1.81 |
| Use | This product is for scientific research only and shall not be used for other purposes. |
117007-52-0 - Risk and Safety
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37/39 - Wear suitable gloves and eye/face protection |
| UN IDs | UN2811 |
117007-52-0 - Reference Information
| Use | 3-iodo-1H-pyrazolo [3,4-B] pyridine is an organic intermediate, which can be obtained by 1H-pyrazolo [3,4-b] pyridine iodide. There are reports that it can be used to prepare compound 3-(2-{[6-(trifluoromethyl) pyridine -3-yl] oxy} pyridine -3-yl) pyrazolo [1,5-a] pyridine. |
| preparation | pyrazolo [1,5-a] pyridine (M-5)(300 mg, 2.54 mmol) was dissolved in acetonitrile (5.0 mL), NIS(628 mg, 2.79 mmol) was added, and the mixture was stirred at room temperature for 1 hour. After filtration, the solvent is evaporated under reduced pressure. The residue was purified by silica gel column chromatography (n-hexane: ethyl acetate) to give the compound 3-iodo-1H-pyrazolo [3,4-B] pyridine as a pale yellow solid (556 mg, 90%). |
Last Update：2024-04-09 19:05:05
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