268731-07-3

268731-07-3 - Names and Identifiers

Name	Fmoc-D-1,2,3,4-Tetrahydronorharman-3-carboxylic acid
Synonyms	FMOC-D-TPI FMOC-D-TPI-OH Fmoc-D-Tpi-OH FMOC-D-THNH(3)-OH FMOC-D-1,2,3,4-TETRAHYDRONORHARMAN-3-CARBOXYLIC ACID Fmoc-D-1,2,3,4-Tetrahydronorharman-3-carboxylic acid N-ALPHA-(9-FLUORENYLMETHOXYCARBONYL)-D-TRYPTOLINE-3-CARBOXYLIC ACID (R)-1,2,3,4-Tetrahydronorharman-3-carboxylic acid, N2-FMOC protected FMOC-D-1,2,3,4-TETRAHYDRO-9H-PYRIDO-[3,4-B]-INDOLE-3-CARBOXYLIC ACID N-ALPHA-(9-FLUORENYLMETHOXYCARBONYL)-D-1,2,3,4-TETRAHYDRONORHARMAN-3-CARBOXYLIC ACID (3R)-2-[(9H-fluoren-9-ylmethoxy)carbonyl]-2,3,4,9-tetrahydro-1H-beta-carboline-3-carboxylic acid
CAS	268731-07-3
InChI	InChI=1/C27H22N2O4/c30-26(31)25-13-21-20-11-5-6-12-23(20)28-24(21)14-29(25)27(32)33-15-22-18-9-3-1-7-16(18)17-8-2-4-10-19(17)22/h1-12,22,25,28H,13-15H2,(H,30,31)/t25-/m1/s1

268731-07-3 - Physico-chemical Properties

Molecular Formula	C27H22N2O4
Molar Mass	438.47
Density	1.396±0.06 g/cm3(Predicted)
Boling Point	702.4±60.0 °C(Predicted)
Flash Point	378.6°C
Vapor Presure	1.04E-20mmHg at 25°C
pKa	3.92±0.20(Predicted)
Storage Condition	Store at -15°C
Refractive Index	1.713

268731-07-3 - Risk and Safety

Hazard Symbols	Xi - Irritant
HS Code	29242990
Hazard Class	IRRITANT

268731-07-3 - Introduction

Fmoc-D-1,2,3, acid is a chemical compound, its chemical formula is C34H29NO4, molecular weight is 511.60. It is an amino acid derivative containing a Fmoc protecting group and has the structure of tetrahydro-beta-carboline and formic acid. The following is an introduction to its nature, use, preparation and safety information:

Nature:
-Appearance: White or off-white crystalline solid
-Melting point: about 165-170 ° C
-Insoluble in water, soluble in organic solvents such as dichloromethane and dimethyl sulfoxide

Use:
Fmoc-D-1,2,3, acid is widely used in the field of organic synthesis, often used in the synthesis of peptide compounds or drugs, as part of amino acid residues.

Method:
Fmoc-D-1,2,3, acid can be synthesized by the following steps:
1. D-1,2,3, 4-tetrahydro-β-carboline-3-carboxylic acid was reacted with chloromethyl dimethyl-n-butyl ammonium salt to generate 1,2,3, 4-Tetrahydro-β-carboline-3-carboxylic acid
2.1,2, 3,4-tetrahydro-β-carboline-3-carboxylic acid reacts with Fmoc-Cl to produce N-Fmoc-D-1,2,3, 4-Tetrahydro-β-carboline-3-carboxylic acid

Safety Information:
Fmoc-D-1,2,3, acid is a chemical, and you need to pay attention to safe operation when using it. It may cause irritation to the eyes, skin and respiratory tract, so you should wear appropriate protective measures, such as laboratory coats, protective glasses and gloves. In addition, it should be operated in a well-ventilated area to avoid inhaling the vapors of the substance. If skin contact or inhalation occurs, rinse immediately with water and seek medical help.

Last Update：2024-04-09 20:49:11

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