26908-82-7

26908-82-7 - Names and Identifiers

Name	(4-Methylphenyl)sulfonyl acetate
Synonyms	p-tolylsulfonyl acetate acetyl p-toluenesulfonate UOAJUPONZOXFNX-UHFFFAOYSA-N (4-Methylphenyl)sulfonyl acetate (4-METHYLPHENYL)SULFONYL ACETATE (4-Methylbenzene)sulfonyl Acetate Acetic P-Toluenesulfonic Anhydride Acetic Acid, Anhydride With P-Toluenesulfonic Acid Acetic acid, anhydride with 4-methylbenzenesulfonic acid
CAS	26908-82-7
InChI	InChI=1/C9H10O4S/c1-7-3-5-9(6-4-7)14(11,12)13-8(2)10/h3-6H,1-2H3

26908-82-7 - Physico-chemical Properties

Molecular Formula	C9H10O4S
Molar Mass	214.24
Density	1.279±0.06 g/cm3(Predicted)
Boling Point	325.7±35.0 °C(Predicted)
Flash Point	150.8°C
Vapor Presure	0.000227mmHg at 25°C
Refractive Index	1.524

26908-82-7 - Reference Information

production method

(1) reflux dry p-toluenesulfonic acid with excess acetyl chloride for 3~5h until no hydrogen chloride gas is released. The excess acetyl chloride is evaporated under reduced pressure to obtain the colorless crystalline mixed anhydride product. (2) Mix dry p-toluenesulfonic acid with excess acetic anhydride evenly, heat at 130 ℃ for 30min, and then steam the acetic acid and excess acetic anhydride under reduced pressure at 70 ℃. The residue is the obtained mixed anhydride product. The mixed anhydride of the above two methods contains 6% ~ 10% p-toluenesulfonic acid and 5% ~ 20% p-toluenesulfonic acid anhydride, and can be used without further purification

Last Update：2024-04-09 21:11:58