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3141-24-0

2,3,5-Tribromothiophene

CAS: 3141-24-0

Molecular Formula: C4HBr3S

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3141-24-0 - Names and Identifiers

Name 2,3,5-Tribromothiophene
Synonyms S0507
AI3-62838
NSC 263503
2,3,5-Tribromothioph
2,3,5-Tribromothiophene
2,3,5-tribromo-thiophen
2,3,5-TRIBROMOTHIOPHENE
Thiophene,2,3,5-tribromo-
Thiophene, 2,3,5-tribromo-
CAS 3141-24-0
EINECS 221-544-7
InChI InChI=1/C4HBr3S/c5-2-1-3(6)8-4(2)7/h1H

3141-24-0 - Physico-chemical Properties

Molecular FormulaC4HBr3S
Molar Mass320.83
Density2.483 g/mL at 25 °C (lit.)
Melting Point25-28 °C (lit.)
Boling Point120 °C/11 mmHg (lit.)
Flash Point>230°F
Vapor Presure0.0203mmHg at 25°C
Appearancesolid
Specific Gravity2.483
BRN111486
Storage ConditionKeep in dark place,Inert atmosphere,2-8°C
Refractive Indexn20/D 1.664(lit.)

3141-24-0 - Risk and Safety

Risk CodesR20/21/22 - Harmful by inhalation, in contact with skin and if swallowed.
R36/37/38 - Irritating to eyes, respiratory system and skin.
Safety DescriptionS36/37/39 - Wear suitable protective clothing, gloves and eye/face protection.
S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
UN IDsUN 2929 6.1/PG 2
WGK Germany3
TSCAT
HS Code29349990
Hazard Class6.1

3141-24-0 - Reference Information

production method 80mL chloroform and 168.2g thiophene are added into the reactor, 960g of liquid bromine is slowly added dropwise at 30 ℃ and under stirring, the reaction starts immediately and a large amount of hydrogen bromide gas escapes, and the dropwise addition is completed in about 4 hours. The reactants are heated and refluxed for 2h, cooled to room temperature, 50 mL2mol/L sodium hydroxide and 205mL 95% ethanol are added to the reactants respectively, and stirred for 10min. Inject the reaction mixture into 400mL of water to separate the organic phase, dry with anhydrous magnesium sulfate, filter, and evaporate the solvent in the filtrate. 423.6g of fraction at 109~110 ℃(95.2Pa) was collected by vacuum distillation with 66% yield.
EPA chemical information information provided by: ofmpub.epa.gov (external link)
Last Update:2024-04-10 22:29:15
3141-24-0
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Email: 3623107365@qq.com
Mobile: 18916960931
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