5211-62-1
2-Methoxyphenylacetone
CAS: 5211-62-1
Molecular Formula: C10H12O2
5211-62-1 - Names and Identifiers
| Name | 2-Methoxyphenylacetone |
| Synonyms | O-ANISYLACETONE o-Acetonylanisole 2-Methoxyphenylacetone O-METHOXYPHENYL ACETONE 1-(2-Methoxyphenyl)acetone 2-Methoxybenzyl methyl ketone 2-METHOXYBENZYL METHYL KETONE O-METHOXY BENZYL METHYL KETONE 1-(2-METHOXYPHENYL)-2-PROPANONE 1-(2-Methoxyphenyl)-2-propanone 1-(2-methoxyphenyl)propan-2-one 2-Propanone, 1-(2-methoxyphenyl)- |
| CAS | 5211-62-1 |
| EINECS | 226-008-6 |
| InChI | InChI=1/C10H12O2/c1-8(11)7-9-5-3-4-6-10(9)12-2/h3-6H,7H2,1-2H3 |
5211-62-1 - Physico-chemical Properties
| Molecular Formula | C10H12O2 |
| Molar Mass | 164.2 |
| Density | 1.054g/mLat 25°C(lit.) |
| Melting Point | 127-130°C (10 mmHg) |
| Boling Point | 127-130°C10mm Hg(lit.) |
| Flash Point | >230°F |
| Solubility | Chloroform (Slightly), Ethyl Acetate (Slightly) |
| Vapor Presure | 0.0114mmHg at 25°C |
| Appearance | Oil |
| Color | Clear Colourless |
| BRN | 2502308 |
| Storage Condition | -20°C Freezer |
| Refractive Index | n20/D 1.525(lit.) |
| MDL | MFCD00008770 |
| Physical and Chemical Properties | Liquid. Boiling point 1248-130 ℃(1.87kpa), relative density 1.054, refractive index (nD20)1.5250. |
5211-62-1 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Safety Description | S24/25 - Avoid contact with skin and eyes. |
| WGK Germany | 3 |
| HS Code | 29145000 |
| Hazard Note | Irritant |
5211-62-1 - Reference Information
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| uses | intermediates of the adrenergic drug methoxyphenamine. |
| production method | o-methoxybenzaldehyde is obtained by condensation, reduction and hydrolysis. Stir and mix o-methoxybenzaldehyde, nitroethane, toluene and n-butylamine, and steam out toluene and water until the dehydration amount reaches the theoretical value. Then add water, iron powder and ferric chloride, heat up to reflux, and add hydrochloric acid dropwise. After dropping, keep reflux for 1h, filter, and extract with toluene. The extract was washed with sodium bisulfite, distilled under reduced pressure, and the fraction at 128 ℃(2.0kPa) was collected to obtain 2-methoxyphenylacetone. 53% yield. |
Last Update：2024-04-09 20:45:29
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