6023-29-6
2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1)
CAS: 6023-29-6
Molecular Formula: C14H20N3O3.1/2Cl4Zn
6023-29-6 - Names and Identifiers
| Name | 2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1) |
| Synonyms | 2,5-Diethoxy-4-Morpholinobenzenediazonium Tetrachlorozincate |
| CAS | 6023-29-6 |
| EINECS | 2278800 |
6023-29-6 - Physico-chemical Properties
| Molecular Formula | C14H20N3O3.1/2Cl4Zn |
| Molar Mass | 485.51 |
6023-29-6 - Introduction
2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1) is an organic compound with the chemical formula C12H16Cl4N4O2Zn.
Nature:
-Appearance: White crystalline solid
-Melting point: 132-135 degrees Celsius
-Solubility: Soluble in organic solvents, such as benzene, carbon disulfide and ethanol, slightly soluble in water.
Use:
- 2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1) is an organic zinc reagent that can be used in organic synthesis reactions, such as the rearrangement, coupling and cyclization of carbonyl compounds.
-can also be used as dehydration reagent, dehydration reducing agent and pyridine base catalyst.
Method: The preparation of
2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1) generally uses the following steps:
1. morpholine reacts with zinc tetrachloride to produce morpholine zinc tetrachloride;
2. morpholine zinc tetrachloride reacts with p-cresol alcohol to generate 2,5-diethoxy -4-(morpholin-4-yl) benzene.
3.2,5-diethoxy-4-(morpholin-4-yl)benzene was reacted with zinc tetrachloride to obtain the target product, 2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1).
Safety Information:
2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium the toxicity of tetrachlorozincate (2:1) is low, the following safety measures should still be paid attention:
-Avoid inhaling aerosols or dust, and wear respiratory protective equipment when using;
-Avoid contact with skin and eyes, wear chemical protective gloves and goggles when using;
-avoid ingestion, avoid eating, drinking water and smoking, etc;
-Maintain good ventilation conditions during operation to avoid the accumulation of harmful gases;
-Store away from fire and oxidizing agents and keep containers sealed.
Nature:
-Appearance: White crystalline solid
-Melting point: 132-135 degrees Celsius
-Solubility: Soluble in organic solvents, such as benzene, carbon disulfide and ethanol, slightly soluble in water.
Use:
- 2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1) is an organic zinc reagent that can be used in organic synthesis reactions, such as the rearrangement, coupling and cyclization of carbonyl compounds.
-can also be used as dehydration reagent, dehydration reducing agent and pyridine base catalyst.
Method: The preparation of
2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1) generally uses the following steps:
1. morpholine reacts with zinc tetrachloride to produce morpholine zinc tetrachloride;
2. morpholine zinc tetrachloride reacts with p-cresol alcohol to generate 2,5-diethoxy -4-(morpholin-4-yl) benzene.
3.2,5-diethoxy-4-(morpholin-4-yl)benzene was reacted with zinc tetrachloride to obtain the target product, 2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium tetrachlorozincate (2:1).
Safety Information:
2,5-diethoxy-4-(morpholin-4-yl)benzenediazonium the toxicity of tetrachlorozincate (2:1) is low, the following safety measures should still be paid attention:
-Avoid inhaling aerosols or dust, and wear respiratory protective equipment when using;
-Avoid contact with skin and eyes, wear chemical protective gloves and goggles when using;
-avoid ingestion, avoid eating, drinking water and smoking, etc;
-Maintain good ventilation conditions during operation to avoid the accumulation of harmful gases;
-Store away from fire and oxidizing agents and keep containers sealed.
Last Update：2024-04-10 22:29:15
