83647-42-1
3-Amino-2-Methylbenzyl Alcohol
CAS: 83647-42-1
Molecular Formula: C8H11NO
83647-42-1 - Names and Identifiers
83647-42-1 - Physico-chemical Properties
| Molecular Formula | C8H11NO |
| Molar Mass | 137.18 |
| Density | 1.126±0.06 g/cm3(Predicted) |
| Melting Point | 106-108 °C (lit.) |
| Boling Point | 300.8±27.0 °C(Predicted) |
| Appearance | Powder |
| Color | Off-white to light orange/purple |
| pKa | 14.53±0.10(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
83647-42-1 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37/39 - Wear suitable gloves and eye/face protection |
| WGK Germany | 3 |
83647-42-1 - Reference Information
| use | 3-amino -2-methylbenzyl alcohol can be used as an intermediate in pharmaceutical synthesis. |
| preparation | iron powder (183mg,3.29mmol) and ammonium chloride (22mg,0.419mmol) were added to the solution of stirred (2-methyl -3-nitro-phenyl)-methanol (13)(100mg,0.598mmol) in EtOH(5mL) and water (1mL), and the obtained mixture was refluxed for 2 hours. The reaction mixture was then raised to room temperature and filtered through a bed of diatomaceous earth. The filtrate was diluted with EtOAc, washed with water, dried and concentrated with sodium sulfate under reduced pressure to obtain 3-amino-2-methylbenzyl alcohol (70mg,85%), which was a yellow jelly. |
Last Update：2024-04-09 21:11:58
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