N-Boc-3-aminomethylmorpholine
N-Boc-3-aminomethylmorpholine
CAS: 475106-18-4
Molecular Formula: C10H20N2O3
N-Boc-3-aminomethylmorpholine - Names and Identifiers
N-Boc-3-aminomethylmorpholine - Physico-chemical Properties
| Molecular Formula | C10H20N2O3 |
| Molar Mass | 216.28 |
| Density | 1.078±0.06 g/cm3(Predicted) |
| Boling Point | 310.7±27.0 °C(Predicted) |
| Flash Point | 141.7°C |
| Vapor Presure | 0.000589mmHg at 25°C |
| pKa | 10.01±0.29(Predicted) |
| Storage Condition | 2-8°C(protect from light) |
| Refractive Index | 1.477 |
N-Boc-3-aminomethylmorpholine - Reference Information
| use | 3-aminomethyl-morpholine -4-butyl carbonate can be used as an intermediate in pharmaceutical synthesis. |
| preparation | will 3-[(2,2, the mixture of 2-trifluoroethanoamino)-methyl]-morpholin-4-carboxylic acid tert-butyl ester (1.7g) and potassium carbonate (3.77g) in methanol (80ml) and water (27ml) was stirred at ambient temperature for 4 hours, and then heated at 50°C for 2 hours. The reaction mixture was concentrated to remove methanol, diluted with water and extracted with ethyl acetate (x3) and dichloromethane (x4). The combined extract was dried and evaporated to obtain the title product 3-aminomethylmorpholin-4-tert-butyl carbonate (0.97g), which was a yellow jelly. |
Last Update：2024-04-10 22:29:15
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CAS: 475106-18-4
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CAS: 475106-18-4
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