TriMethyl(broModifluoroMethyl)silane
TriMethyl(broModifluoroMethyl)silane
CAS: 115262-01-6
Molecular Formula: C4H9BrF2Si
TriMethyl(broModifluoroMethyl)silane - Names and Identifiers
| Name | TriMethyl(broModifluoroMethyl)silane |
| Synonyms | (Bromodifluoromethyl) TriMethyl(broModifluoroMethyl)silane Bromodifluoro(trimethylsilyl)methane (BroModifluoroMethyl)triMethylsilane Silane, (bromodifluoromethyl)trimethyl- |
| CAS | 115262-01-6 |
| EINECS | 806-938-4 |
| InChIKey | WDZVWBWAUSUTTO-UHFFFAOYSA-N |
TriMethyl(broModifluoroMethyl)silane - Physico-chemical Properties
| Molecular Formula | C4H9BrF2Si |
| Molar Mass | 203.1005664 |
| Density | 1.306 |
| Boling Point | 108°C(lit.) |
| Flash Point | 46℃ |
| Appearance | Form liquid, color clear |
| Storage Condition | -20°C |
| Refractive Index | n/D1.407 |
| Use | Use difluoromethyltrimethylsilane is an organic intermediate, which has been reported to be useful in the preparation of its derivatives. |
TriMethyl(broModifluoroMethyl)silane - Risk and Safety
| Risk Codes | 11 - Highly Flammable |
| Safety Description | 24/25 - Avoid contact with skin and eyes. |
| UN IDs | UN 1993C 3 / PGIII |
| TSCA | No |
| HS Code | 29319090 |
| Hazard Class | 3 |
| Packing Group | II |
TriMethyl(broModifluoroMethyl)silane - Upstream Downstream Industry
TriMethyl(broModifluoroMethyl)silane - Preparation
Fill the flask equipped with reflux condenser with NaBr (10.8g, 105 mmol), 30% H2O2 aqueous solution (14.2g, 125 mmol) and water (7 mL). The mixture was cooled in an ice/water bath and concentrated sulfuric acid (6.7mL,125mmol) was added dropwise. Remove the cooling bath and add TMSCHF2 (12.4g,100mmol) to the resulting dark mixture. The reaction flask was immersed in a 40°C water bath and stirred at this temperature under the irradiation of a household incandescent bulb (75W) until the bromine color almost disappeared (about 1 hour). The upper phase was separated, filtered through MgSO4 and distilled. Colorless liquid, yield 16.2g,80%.
Last Update：2024-04-10 22:29:15
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View History
Raw Materials for TriMethyl(broModifluoroMethyl)silane
(chlorodifluoroMethyl)triMethylsilane
DIBROMODIFLUOROMETHANE
(Difluoromethyl)trimethylsilane
Bromotrimethylsilane
(Trifluoromethyl)trimethylsilane
Chlorotrimethylsilane
DIBROMODIFLUOROMETHANE
(Difluoromethyl)trimethylsilane
Bromotrimethylsilane
(Trifluoromethyl)trimethylsilane
Chlorotrimethylsilane
Downstream Products for TriMethyl(broModifluoroMethyl)silane