(2-羟基-1,1-二甲基乙基)氨基甲酸叔丁酯
N-Boc-2-Amino-2-Methyl-1-Propanol
CAS: 102520-97-8
Molecular Formula: C9H19NO3
(2-羟基-1,1-二甲基乙基)氨基甲酸叔丁酯 - Names and Identifiers
(2-羟基-1,1-二甲基乙基)氨基甲酸叔丁酯 - Physico-chemical Properties
| Molecular Formula | C9H19NO3 |
| Molar Mass | 189.25 |
| Density | 1.012±0.06 g/cm3(Predicted) |
| Melting Point | 57-62 °C |
| Boling Point | 286.5±23.0 °C(Predicted) |
| Flash Point | 127.097°C |
| Vapor Presure | 0mmHg at 25°C |
| pKa | 12.24±0.46(Predicted) |
| Storage Condition | 2-8°C |
| Refractive Index | 1.453 |
| Physical and Chemical Properties | WGK Germany:2 |
(2-羟基-1,1-二甲基乙基)氨基甲酸叔丁酯 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
| WGK Germany | 2 |
(2-羟基-1,1-二甲基乙基)氨基甲酸叔丁酯 - Introduction
N-Boc-2-Amino -2-methyl -1-propanol is an organic compound, often abbreviated as Boc-APC. The following is a description of its nature, use, preparation and safety information:
Nature:
N-Boc-2-Amino -2-methyl -1-propanol is a solid compound with the chemical formula C9H19NO3. It has a colorless or white crystalline form and is deliquescent. The compound has a density of about 1.08g/cm³ and a melting point of about 75-78 degrees Celsius.
Use:
N-Boc-2-Amino -2-methyl -1-propanol is widely used in organic synthesis to prepare a variety of compounds. It is often used as a protecting group capable of protecting the amine function to which it is attached. It can be removed from the target compound by a deprotection reaction. In addition, it can also be used as an intermediate in the synthesis of drugs, natural products and other organic synthesis reactions.
Preparation Method:
The preparation method of N-Boc-2-amino -2-methyl -1-propanol is mainly carried out through the following steps: first, 2-amino -2-methyl -1-propanol and dimethylaminopropanol (DMAP) are reacted under alkaline conditions to obtain an intermediate; then, phthalic anhydride (N-Boc-OSu) is used to react with the intermediate to form N-Boc-2-amino -2-methyl -1-propanol; finally, the pure product was obtained by purification methods such as crystallization or column chromatography.
Safety Information:
N-Boc-2-amino -2-methyl -1-propanol is an organic compound, which is relatively stable under general conditions. However, it is a deliquescent compound and should be kept away from humid air and moisture. In addition, it has an irritating effect on the eyes, skin and the respiratory tract of the human body. Appropriate laboratory safety measures should be taken when handling and using the compound, such as wearing protective glasses, laboratory clothing and gloves, and ensuring good ventilation.
Nature:
N-Boc-2-Amino -2-methyl -1-propanol is a solid compound with the chemical formula C9H19NO3. It has a colorless or white crystalline form and is deliquescent. The compound has a density of about 1.08g/cm³ and a melting point of about 75-78 degrees Celsius.
Use:
N-Boc-2-Amino -2-methyl -1-propanol is widely used in organic synthesis to prepare a variety of compounds. It is often used as a protecting group capable of protecting the amine function to which it is attached. It can be removed from the target compound by a deprotection reaction. In addition, it can also be used as an intermediate in the synthesis of drugs, natural products and other organic synthesis reactions.
Preparation Method:
The preparation method of N-Boc-2-amino -2-methyl -1-propanol is mainly carried out through the following steps: first, 2-amino -2-methyl -1-propanol and dimethylaminopropanol (DMAP) are reacted under alkaline conditions to obtain an intermediate; then, phthalic anhydride (N-Boc-OSu) is used to react with the intermediate to form N-Boc-2-amino -2-methyl -1-propanol; finally, the pure product was obtained by purification methods such as crystallization or column chromatography.
Safety Information:
N-Boc-2-amino -2-methyl -1-propanol is an organic compound, which is relatively stable under general conditions. However, it is a deliquescent compound and should be kept away from humid air and moisture. In addition, it has an irritating effect on the eyes, skin and the respiratory tract of the human body. Appropriate laboratory safety measures should be taken when handling and using the compound, such as wearing protective glasses, laboratory clothing and gloves, and ensuring good ventilation.
Last Update：2024-04-09 21:01:54
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CAS: 102520-97-8
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