(Trimethylsiloxymethyl)benzene

Name	BENZYLOXYTRIMETHYLSILANE
Synonyms	BENZYLOXYTRIMETHYLSILANE Benzyl (trimethylsilyl) ether Silane, (benzyloxy)trimethyl- (Trimethylsiloxymethyl)benzene Phenyl(trimethylsilyloxy)methane Silane, trimethyl(phenylmethoxy)- Benzyl trimethylsilyl ether, Trimethylbenzyloxysilane Benzyl trimethylsilyl ether, Trimethylbenzyloxysilane
CAS	14642-79-6
InChI	InChI=1/C10H16OSi/c1-12(2,3)11-9-10-7-5-4-6-8-10/h4-8H,9H2,1-3H3

Molecular Formula	C10H16OSi
Molar Mass	180.32
Density	0.916
Boling Point	92 °C
Flash Point	73°C
Solubility	Chloroform, Dichloromethane
Vapor Presure	0.373mmHg at 25°C
Appearance	Yellow Liquid
Specific Gravity	0.916
Color	Colorless to Light yellow to Light red
Storage Condition	Room Temprature
Sensitive	7: reacts slowly with moisture/water
Refractive Index	1.4770

Risk Codes	36/37/38 - Irritating to eyes, respiratory system and skin.
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S24/25 - Avoid contact with skin and eyes. S23 - Do not breathe vapour.
TSCA	No
HS Code	29310099

NIST chemical information	Information provided by: webbook.nist.gov (external link)
use	benzyloxytrimethylsilane is a kind of silane compound and can be used as an intermediate in pharmaceutical synthesis.
Preparation	The preparation of benzyloxytrimethylsilane is as follows: Under solvent-free conditions, benzyl alcohol (1mmol) is added to HMDS(1mmol) and The mixture of MNPs-DABCO tribromide (10mg), and then the mixture is stirred at room temperature for a specified time. Monitoring progress through TLC. After the reaction is complete, the catalyst is separated from the product (within 5 seconds) and washed with Et2O(2 × 5mL). 10% NaHCO3 aqueous solution (3mL) was added to destroy the amount of additional HMDS, then the organic layer was separated and dried with anhydrous Na2SO4. Evaporation and decompression under Et2O makes pure TMS-ether without additional purification to obtain benzyloxytrimethylsilane.

Last Update：2024-04-10 22:29:15

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(Trimethylsiloxymethyl)benzene

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