-Bromoethylphthalimide
N-(2-Bromoethyl)phthalimide
CAS: 574-98-1
Molecular Formula: C10H8BrNO2
-Bromoethylphthalimide - Names and Identifiers
-Bromoethylphthalimide - Physico-chemical Properties
| Molecular Formula | C10H8BrNO2 |
| Molar Mass | 254.08 |
| Density | 1.6254 (rough estimate) |
| Melting Point | 80-83 °C (lit.) |
| Boling Point | 318 °C |
| Flash Point | 161.2°C |
| Water Solubility | insoluble |
| Vapor Presure | 7.3E-05mmHg at 25°C |
| Appearance | Crystalline Powder |
| Color | White to slightly pink or beige |
| BRN | 148736 |
| pKa | -2.35±0.20(Predicted) |
| Storage Condition | Sealed in dry,Room Temperature |
| Refractive Index | 1.6320 (estimate) |
| MDL | MFCD00005902 |
| Physical and Chemical Properties | White powder |
-Bromoethylphthalimide - Risk and Safety
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | 24/25 - Avoid contact with skin and eyes. |
| WGK Germany | 3 |
| TSCA | Yes |
| HS Code | 29251995 |
-Bromoethylphthalimide - Reference Information
| NIST chemical information | information provided by: webbook.nist.gov (external link) |
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| Use | pharmaceutical intermediates. for synthesis of inorganic ligands |
| production method | N-(2-bromoethyl) phthalimide can be synthesized from phthalic anhydride by condensation and bromination: phthalic anhydride was added to the reaction pan, and ethanolamine was slowly added thereto. The mixture was heated to 110 ° C. And distilled to remove water, followed by vacuum drying for 2 hours. Phosphorus tribromide was added dropwise at 110-120 ° C. After addition, the mixture was kept and stirred for 1.5h. It is cooled to 80 ° C., charged into crushed ice, decomposed excess phosphorus tribromide, left standing overnight, crystallized, centrifuged and dried, then recrystallized with ethanol, and dried at about 60 ° C. To obtain a finished product. |
Last Update：2024-04-09 02:00:09
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