1-(2-羟基-6-甲氧基苯基)乙基-1-酮
2'-HYDROXY-6'-METHOXYACETOPHENONE
CAS: 703-23-1
Molecular Formula: C9H10O3
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Names and Identifiers
| Name | 2'-HYDROXY-6'-METHOXYACETOPHENONE |
| Synonyms | 2'-HYDROXY-6'-METHOXYACETOPHEN 2-HYDROXY-6-METHOXYACETOPHENONE 2'-HYDROXY-6'-METHOXYACETOPHENONE 6'-Hydroxy-2'-methoxyacetophenone 2'-Hydroxy-6'-methoxyacetophenone Acetophenone, 2'-hydroxy-6'-methoxy- 1-(2-HYDROXY-6-METHOXYPHENYL)ETHANONE 1-(2-HYDROXY-6-METHOXYPHENYL)ETHAN-1-ONE |
| CAS | 703-23-1 |
| EINECS | 211-872-9 |
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Physico-chemical Properties
| Molecular Formula | C9H10O3 |
| Molar Mass | 166.17 |
| Density | 1.158 |
| Melting Point | 58-60°C(lit.) |
| Boling Point | 141°C16mm Hg(lit.) |
| Flash Point | 141°C/16mm |
| BRN | 1869049 |
| pKa | 9.79±0.10(Predicted) |
| Storage Condition | Sealed in dry,Room Temperature |
| Refractive Index | 1.5500 (estimate) |
| MDL | MFCD00008732 |
| Use | Application 1-(2-hydroxy-6-methoxyphenyl) ethyl -1-one is an organic intermediate that can be obtained by methylation of 2, 6-dihydroxyacetophenone, the methylating reagent can be selected from dimethyl sulfate and methyl iodide, and is mainly used in laboratory research and development process and chemical production process. |
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Risk and Safety
| Hazard Symbols | Xi - Irritant |
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37/39 - Wear suitable gloves and eye/face protection |
| WGK Germany | 3 |
| TSCA | N |
| HS Code | 29145090 |
| Hazard Note | Irritant |
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Upstream Downstream Industry
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Preparation
10.00g 2,6-dihydroxyacetophenone is dissolved in 80mL anhydrous acetone, stirred in a round bottom flask for 5min, 9.991g anhydrous potassium carbonate is added for 10min, 9.120g dimethyl sulfate is added dropwise in a constant pressure drop funnel for 30min, reflux reaction is performed for 6h, cooling to room temperature, adjusting PH value to 2 with hydrochloric acid, extracting organic phase, after that, column chromatography V (petroleum ether):V (ethyl acetate) = 10:1 was carried out to obtain colorless liquid 1-(2-hydroxy-6-methoxyphenyl) ethyl-1-one (9.894g yield 90.65%).
Last Update：2024-04-10 22:29:15
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Security information
| WGK Germany | 3 |
| Hazard Note | Irritant |
| TSCA | N |
| customs code | 29145090 |
Last Update：2024-04-09 20:45:29
1-(2-羟基-6-甲氧基苯基)乙基-1-酮 - Reference Information
| Application | 1-(2-hydroxy-6-methoxyphenyl) ethyl -1-One is an organic intermediate, which can be obtained by methylation of 2, 6-dihydroxyacetophenone. The methylation reagent can be selected from dimethyl sulfate and methyl iodide, it is mainly used in laboratory research and development process and chemical production process. |
| preparation | 10.00g of 2,6-dihydroxyacetophenone is dissolved in 80mL of anhydrous acetone, stirred in a round bottom flask for 5min, 9.991g of anhydrous potassium carbonate is added and stirred for 10min, 9.120g of dimethyl sulfate is dropwise in a constant pressure drip funnel for 30min, reflux reaction for 6h, and cooling to room temperature, adjust the PH value to 2 with hydrochloric acid, extract the organic phase with ethyl acetate, wash the organic phase with water and saturated salt water in turn, dry with anhydrous sodium sulfate, and then perform column chromatography V (petroleum ether):V (ethyl acetate) = 10:1 to obtain colorless liquid 1-(2-hydroxy-6-methoxyphenyl) ethyl -1-one (9.894g yield 90.65%). |
Last Update：2024-04-09 20:52:54
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Product Name: 1-(2-Hydroxy-6-methoxyphenyl)ethanone Visit Supplier Webpage Request for quotationCAS: 703-23-1
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Mobile: +86-18621343501
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Product Name: 2'-Hydroxy-6'-methoxyacetophenone Visit Supplier Webpage Request for quotationCAS: 703-23-1
Tel: +86-18821248368
Email: Int06@meryer.com
Mobile: +86-18821248368
QQ: 495145328
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Spot supply
Product Name: 1-(2-Hydroxy-6-Methoxyphenyl)ethanone Visit Supplier Webpage Request for quotationCAS: 703-23-1
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View History
1-(2-羟基-6-甲氧基苯基)乙基-1-酮
更昔洛韦杂质H(EP)
2,6-DIFLUOROBENZOIC ACID
DROFENINE HYDROCHLORIDE
[2-(三氟甲氧基)苯基]肼盐酸盐
甲氧基乙氧基乙基甲基丙烯酸酯
Phosphoric acid 2-ethylhexyl ester
槲皮素 3-O-葡萄糖基 (1→2)鼠李糖苷
磺基琥珀酸单异癸酯二钠
ADENOSINE-3(+2')-MONOPHOSPHORIC ACID MONOHYDRATE*
更昔洛韦杂质H(EP)
2,6-DIFLUOROBENZOIC ACID
DROFENINE HYDROCHLORIDE
[2-(三氟甲氧基)苯基]肼盐酸盐
甲氧基乙氧基乙基甲基丙烯酸酯
Phosphoric acid 2-ethylhexyl ester
槲皮素 3-O-葡萄糖基 (1→2)鼠李糖苷
磺基琥珀酸单异癸酯二钠
ADENOSINE-3(+2')-MONOPHOSPHORIC ACID MONOHYDRATE*
Raw Materials for 1-(2-羟基-6-甲氧基苯基)乙基-1-酮
3-METHOXY-2-(TRIMETHYLSILYL)PHENYL TRIFLUOROMETHANESULFONATE,95.0+%(GC)
2-acetyl-3-hydroxycyclohex-2-enone
2',6'-Dihydroxyacetophenone
Dimethyl sulfate
N,N-Dimethylacetamide
Chlorotrimethylsilane
2-acetyl-3-hydroxycyclohex-2-enone
2',6'-Dihydroxyacetophenone
Dimethyl sulfate
N,N-Dimethylacetamide
Chlorotrimethylsilane
Downstream Products for 1-(2-羟基-6-甲氧基苯基)乙基-1-酮