Name | 1-(4-Bromo-2-thienyl)ethan-1-one |
Synonyms | 4-bromo-2-acetylthiophene 1-(4-Bromo-2-thienyl)ethan-1-one 1-(4-bromothiophen-2-yl)ethanone |
CAS | 7209-11-2 |
InChI | InChI=1/C6H5BrOS/c1-4(8)6-2-5(7)3-9-6/h2-3H,1H3 |
Molecular Formula | C6H5BrOS |
Molar Mass | 205.07 |
Density | 1.619g/cm3 |
Boling Point | 284.4°C at 760 mmHg |
Flash Point | 125.8°C |
Vapor Presure | 0.00299mmHg at 25°C |
Storage Condition | Room Temprature |
Refractive Index | 1.583 |
Use | Application 1-(4-bromo-2-thiophene) ethanone can be used as organic synthesis intermediates and pharmaceutical intermediates, mainly used in laboratory research and development process and chemical production process. |
Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. R36 - Irritating to the eyes R22 - Harmful if swallowed |
Safety Description | S24/25 - Avoid contact with skin and eyes. |
HazardClass | IRRITANT |
customs code | 29339900 |
In a 2L three-mouth bottle equipped with a thermometer and a reflux condenser tube, 2-bromothiophene is added, glacial acetic acid and acetic anhydride are added under mechanical stirring, heated and refluxed for 3h, and the reaction is complete. The glacial acetic acid and excess acetic anhydride in the reaction solution are spin-dried, and the gray-white solid is added to the toluene beating, filtered, and dried in a vacuum oven to obtain 2-acetyl-4-bromothiophene.
storage conditions | Keep in dark place,Sealed in dry,2-8°C |