Name | 1-(4-Bromophenyl)-naphthlene |
Synonyms | 1-(4-BroMophenyl)phthalene 1-(4-bromophenyl)naphthalen 1-(4-Bromophenyl)naphthalene 1-(4-Bromophenyl)-naphthlene 1-(4-BROMOPHENYL)-NAPHTHLENE Naphthalene, 1-(4-bromopheny)- 1-(4-Bromophenyl)-naphthalene Naphthalene, 1-(4-bromophenyl)- |
CAS | 204530-94-9 |
EINECS | 812-991-4 |
InChI | InChI=1/C16H11Br/c17-14-10-8-13(9-11-14)16-7-3-5-12-4-1-2-6-15(12)16/h1-11H |
InChIKey | YRPIGRRBBMFFBE-UHFFFAOYSA-N |
Molecular Formula | C16H11Br |
Molar Mass | 283.16 |
Density | 1.381±0.06 g/cm3(Predicted) |
Boling Point | 381.6±11.0 °C(Predicted) |
Flash Point | 182.5°C |
Vapor Presure | 1.1E-05mmHg at 25°C |
Appearance | yellow oil |
Storage Condition | Sealed in dry,Room Temperature |
Refractive Index | 1.667 |
MDL | MFCD07369916 |
Uses | 1-(4-bromophenyl) naphthalene is an aromatic hydrocarbon derivative that can be used as an organic photoelectric intermediate. |
synthesis method | under argon protection, 36.4g of p-dibromobenzene, 40.2g of naphthalene boric acid, 159.6g of potassium phosphate trihydrate, 0.6 g of tris (p-toluene) phosphine, 200 mL of dioxane and 20 mL of water were added to the 500 mL three-mouth bottle. After the argon replacement reaction system, the catalyst Pdz(dba) was added. 0.2g. Control the reaction temperature at 55 ℃, react for 24 hours, quench with water after the reaction is completed by high performance liquid chromatography (HPLC), extract 100mL dichloromethane for 3 times, wash the organic phase with water, separate the organic phase, dry 50g anhydrous magnesium sulfate overnight, filter, and recover the solvent under reduced pressure to obtain 47.6g of 1-(4-bromophenyl) naphthalene. |