Name | 4-T-BUTYL PROPIOPHONE |
Synonyms | 4-T-BUTYL PROPIOPHONE 4-t-butylphenylacetone 1-(4-tert-butylphenyl)propan-2-one 2-Propanone, 1-[4-(1,1-diMethylethyl)phenyl]- |
CAS | 81561-77-5 |
Molecular Formula | C13H18O |
Molar Mass | 190.28 |
Density | 0.939±0.06 g/cm3(Predicted) |
Boling Point | 263.5±9.0 °C(Predicted) |
Physical and Chemical Properties | This product is liquid, insoluble in water, soluble in ketone and benzene solvents. |
use | 4-tert-butylphenylacetone is an intermediate of the fungicide terylene morpholine. |
production method | the preparation method is to add tert-butyl benzene, anhydrous aluminum trichloride and petroleum ether into the reaction kettle, add propionyl chloride dropwise at 20 ℃ for about 2~2.5h under stirring, continue to react for 1h after adding, then pour into ice water, separate the petroleum ether layer, the water layer is extracted with petroleum ether for 1 time, combine petroleum ether liquid, and wash with water, the petroleum ether is recovered by distillation, and then the finished product is distilled under reduced pressure. |