1-BROMO-3-CHLOROBENZENE
3-Bromochlorobenzene
CAS: 108-37-2
Molecular Formula: C6H4BrCl
1-BROMO-3-CHLOROBENZENE - Names and Identifiers
| Name | 3-Bromochlorobenzene |
| Synonyms | m-bromochlorobenzene M-CHLOROBROMOBENZENE 3-Bromochlorobenzene M-BROMOCHLOROBENZENE 3-BROMOCHLOROBENZENE 3-Chlorobromobenzene 1-bromo-3-chloro-benzen 1-BROMO-3-CHLOROBENZENE 1-Chloro-3-bromobenzene 1-bromo-3-chlorobenzene 3-Bromo-1-chlorobenzene 1 -Bromo-3-chloro benzene |
| CAS | 108-37-2 |
| EINECS | 203-575-8 |
| InChI | InChI=1/C6H4BrCl/c7-5-2-1-3-6(8)4-5/h1-4H |
1-BROMO-3-CHLOROBENZENE - Physico-chemical Properties
| Molecular Formula | C6H4BrCl |
| Molar Mass | 191.45 |
| Density | 1.63g/mLat 25°C(lit.) |
| Melting Point | -21.5 °C |
| Boling Point | 196°C(lit.) |
| Flash Point | 177°F |
| Water Solubility | Insoluble |
| Vapor Presure | 0.609mmHg at 25°C |
| Appearance | Liquid |
| Specific Gravity | 1.630 |
| Color | Clear colorless to light yellow |
| BRN | 1446353 |
| Storage Condition | Sealed in dry,Room Temperature |
| Refractive Index | n20/D 1.576(lit.) |
1-BROMO-3-CHLOROBENZENE - Risk and Safety
| Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. R20/22 - Harmful by inhalation and if swallowed. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. S37/39 - Wear suitable gloves and eye/face protection |
| WGK Germany | 3 |
| RTECS | CY9005000 |
| TSCA | Yes |
| HS Code | 29039990 |
| Hazard Note | Irritant |
1-BROMO-3-CHLOROBENZENE - Reference Information
| NIST chemical information | information provided by: webbook.nist.gov (external link) |
| EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
| Use | M-chlorobromobenzene is an organic compound, benzene is a meta hydrogen atom chlorine chlorine bromine substituted products, M-bromochlorobenzene can be used as organic synthesis intermediates and solvents. M-chlorobromobenzene is a reagent for the synthesis of phenols, ethers and benzofurans, and is also used for the preparation of antithrombotic drugs. |
| preparation | with M-chloroaniline as raw material, mixed with concentrated hydrobromic acid, the temperature is reduced to 0 deg C, under stirring, rapid addition of sodium nitrite aqueous solution, O-chloroaniline nitridation, the formation of diazonium salt, in the reaction process should be controlled at a temperature of not more than 10 deg C. Then the Sandmeyer reaction is used, and the catalyst cuprous bromide and hydrobromic acid are added to the reaction system to decompose the diazonium salt. The decomposition reaction is carried out at boiling temperature, M-bromochlorobenzene can be obtained by washing with water, drying to remove water and distillation under reduced pressure. |
Last Update：2024-04-09 21:01:54
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