Name | 1-Bromotetradecane |
Synonyms | 1-Bromtetradecan Myristyl bromide MYRISTYL BROMIDE Bromotetradecane BROMOTETRADECANE Tetradecyl bromide 1-BROMOTETRADECANE 1-Bromotetradecane TETRADECYL BROMIDE 1-tetradecylbromide N-Tetradecyl Bromide N-TETRADECYL BROMIDE 1-Tetradecyl bromide |
CAS | 112-71-0 |
EINECS | 203-999-3 |
InChI | InChI=1/C14H29Br/c1-2-3-4-5-6-7-8-9-10-11-12-13-14-15/h2-14H2,1H3 |
Molecular Formula | C14H29Br |
Molar Mass | 277.28 |
Density | 0.932g/mLat 25°C(lit.) |
Melting Point | 5-6°C(lit.) |
Boling Point | 175-178°C20mm Hg(lit.) |
Flash Point | >230°F |
Water Solubility | insoluble |
Solubility | Chloroform |
Vapor Presure | 0.00131mmHg at 25°C |
Appearance | Liquid |
Color | Clear yellow |
BRN | 1742640 |
Storage Condition | Store below +30°C. |
Stability | Stable. Incompatible with strong bases, strong oxidizing agents. |
Refractive Index | n20/D 1.460(lit.) |
Physical and Chemical Properties | density 0.93 |
Use | For Organic synthesis |
Hazard Symbols | Xi - Irritant |
Risk Codes | R36/37/38 - Irritating to eyes, respiratory system and skin. R22 - Harmful if swallowed |
Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. S24/25 - Avoid contact with skin and eyes. |
WGK Germany | 3 |
TSCA | Yes |
HS Code | 29033036 |
NIST chemical information | information provided by: webbook.nist.gov (external link) |
EPA chemical substance information | information provided by: ofmpeb.epa.gov (external link) |
Use | organic synthesis intermediates. for organic synthesis, can be used for the synthesis of medicine and other fine chemicals. |
production method | is obtained from the bromination of decanol. After the addition of decadiol was added to the reaction Pan, sulfuric acid was added dropwise with stirring, and stirring was continued for half an hour after the addition. Hydrobromic acid was then added and heated to 99-101 °c for 8H. After cooling to 30 ° C., the stirring was stopped and left for 12h, the upper oil was separated and adjusted to pH 8 with 10% sodium carbonate solution. The aqueous layer was separated, and the oil was washed twice with an equal volume of 50% ethanol. The washed oil was added with sodium carbonate, stirred intermittently, and dried for 24 hours. Filtered to obtain the finished product. |