1215387-58-8
5-Bromo-1H-pyrrolo[2,3-c]pyridine
CAS: 1215387-58-8
Molecular Formula: C7H5BrN2
1215387-58-8 - Names and Identifiers
| Name | 5-Bromo-1H-pyrrolo[2,3-c]pyridine |
| Synonyms | 5-BroMo-6-azaindole 5-Bromo-1H-pyrrolo[2,3-c]pyridine 1H-Pyrrolo[2,3-c]pyridine, 5-broMo- |
| CAS | 1215387-58-8 |
| EINECS | 200-589-5 |
1215387-58-8 - Physico-chemical Properties
| Molecular Formula | C7H5BrN2 |
| Molar Mass | 197.03 |
| Density | 1.770 |
| Boling Point | 362.0±22.0 °C(Predicted) |
| pKa | 13.70±0.40(Predicted) |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
1215387-58-8 - Reference Information
| application | 5-bromo-1H-pyrrolo [2,3-C] pyridine is used as an intermediate in organic synthesis and pharmaceutical, mainly used in laboratory research and development process and chemical production process. |
| Preparation | 2-(2-bromo-5-nitropyridine-4-yl)-N,N-dimethylethyl -1-Amino group is dissolved in anhydrous methanol, and a catalytic amount of glacial acetic acid is added, and 70.0 mg (1.10 mmol) sodium cyanoborohydride is weighed in N 2 gas, mix evenly in the flask, stir and heat to 60 ℃, TLC tracks and detects the reaction progress until no reactants are found to stop the reaction, TLC detects (methanol developing agent), and the product Rf = 0.57. The solvent of the reaction mixture is spin-dried, dissolved with dichloromethane, purified water is washed for 2 times, the organic phase is dried with anhydrous sodium sulfate, the mixture is separated by silica gel column chromatography, and the product is vacuum dried to obtain 5-bromo-1H-pyrrolo [2,3-C] pyridine. |
Last Update：2024-04-09 15:16:47
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