185456-26-2 - Names and Identifiers
Name | 1,1,2-Tris(tert-butoxycarbonyl)hydrazine
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Synonyms | BOC3-HYDRAZINE TRIS-BOC-HYDRAZINE TRIS-(T-BUTYLOXYCARBONYL)-HYDRAZINE TRIS-(TERT-BUTYLOXYCARBONYL)-HYDRAZINE 1,1,2-Tris(tert-butoxycarbonyl)hydrazine tri-tert-Butyl hydrazine-1,1,2-tricarboxylate 1,1,2-Hydrazinetricarboxylic acid, 1,1,2-tris(1,1-dimethylethyl) ester Tert-butyl N-[(2-methylpropan-2-yl)oxycarbonyl]-n-[(2-methylpropan-2-yl)oxycarbonylamino]carbamate
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CAS | 185456-26-2
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185456-26-2 - Physico-chemical Properties
Molecular Formula | C15H28N2O6
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Molar Mass | 332.393 |
Density | 1.097±0.06 g/cm3(Predicted) |
Melting Point | 109-110 °C |
Storage Condition | 2-8℃ |
Physical and Chemical Properties | Storage conditions Sealed in dry,2-8°C acidity coefficient (pKa) 7.34±0.50(Predicted) |
Use | This product is for scientific research only and shall not be used for other purposes. |
185456-26-2 - Introduction
1,1,2-Tris(tert-butoxycarbonyl)hydrazine(1,1,2-Tris(tert-butoxycarbonyl)hydrazine) is an organic compound. Its molecular formula is C15H27N3O6 and its molecular weight is 345.39g/mol. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
1,1,2-Tris(tert-butoxycarbonyl)hydrazine is a white solid, soluble in some organic solvents at room temperature. Its melting point is about 76-78°C. The compound is stable, but may decompose at high temperatures.
Use:
1,1,2-Tris(tert-butoxycarbonyl)hydrazine has great potential in organic synthesis. It can be used as a protecting group for the synthesis of other compounds. Because of its high stability and easy removal, it is commonly used in the synthesis of nitrogen-containing compounds, peptides and drugs.
Preparation Method:
1,1,2-Tris(tert-butoxycarbonyl)hydrazine can generally be synthesized by the following steps:
1. with an appropriate amount of tri-tert-butyl carbonyl oxide (tert-butoxycarbonyl chloride) and hydrazine (hydrazine) as reactants.
2. in the absence of solvent or inert solvent (such as dichloromethane) add the appropriate amount of reactants.
3. The reaction is carried out at a suitable temperature, and the common reaction temperature is 0-10°C.
4. The pure 1,1,2-Tris(tert-butoxycarbonyl)hydrazine product can then be obtained by crystallization or other purification methods.
Safety Information:
1,1,2-Tris(tert-butoxycarbonyl)hydrazine is relatively safe under normal conditions of use, but correct laboratory practices still need to be followed. It may be irritating to the eyes and skin, so it is necessary to wear appropriate protective measures when using it, such as laboratory gloves, goggles and protective clothing. In addition, this compound should be kept away from fire and oxidizing agents and stored in a cool, dry place.
Last Update:2024-04-09 20:52:54