1H,1H,2H-PERFLUORO-1-DECENE

1H,1H,2H-PERFLUORO-1-DECENE - Names and Identifiers

Name	3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodec-1-ene
Synonyms	Heptadecafluoro-1-decene (perfluorooctyl)ethylene 1H,1H,2H-Perfluoro-1-Decene 1H,1H,2H-PERFLUORO-1-DECENE 1H,1H,2H-PERFLUORODEC-1-ENE 1,1,2-Trihydroperfluoro-1-decene 1H,1H,2H-HEPTADECAFLUORO-1-DECENE 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodec-1-ene (Perfluoroct-1-yl)ethylene, 3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-Heptadecafluorodec-1-ene
CAS	21652-58-4
EINECS	244-503-5
InChI	InChI=1/C10H3F17/c1-2-3(11,12)4(13,14)5(15,16)6(17,18)7(19,20)8(21,22)9(23,24)10(25,26)27/h2H,1H2
InChIKey	NKAMGQZDVMQEJL-UHFFFAOYSA-N

1H,1H,2H-PERFLUORO-1-DECENE - Physico-chemical Properties

Molecular Formula	C10H3F17
Molar Mass	446.1
Density	1.677 g/mL at 25 °C (lit.)
Boling Point	146-147 °C
Flash Point	>230°F
Water Solubility	Insoluble in water.
Solubility	Chloroform (Sparingly), Methanol (Slightly)
Vapor Presure	6.36mmHg at 25°C
Appearance	Transparent colorless liquid
Specific Gravity	1.677
Color	Colourless
BRN	2066558
Storage Condition	Refrigerator
Refractive Index	n20/D 1.301(lit.)
MDL	MFCD00039246

1H,1H,2H-PERFLUORO-1-DECENE - Risk and Safety

Hazard Symbols	Xi - Irritant
Risk Codes	36/37/38 - Irritating to eyes, respiratory system and skin.
Safety Description	S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing.
UN IDs	1993
WGK Germany	3
TSCA	T
HS Code	29033990
Hazard Note	Harmful
Hazard Class	3.2
Packing Group	III

1H,1H,2H-PERFLUORO-1-DECENE - Reference Information

NIST chemical information	Information provided by: webbook.nist.gov (external link)
EPA chemical information	Information provided by: ofmpub.epa.gov (external link)
application	1H,1H, 2H-perfluoro-1-decene, also known as perfluorooctylethylene, can be used as monomer and chemical intermediate, and can be used in laboratory research and development process and chemical production process.
preparation	perfluorooctane iodide (520g,1.16mmol),Na2S2O4(20.9g,0.12mol),Na2HPO4(21.5g), acetonitrile (900mL) and water (300mL) are added to a 2L autoclave, and ethylene gas is introduced to make the pressure reach 40atm. After 3 hours of continuous reaction at 40-45 ℃, a significant decrease in ethylene pressure was found. 19FNMR tracking reaction found that the raw material has completely reacted, stopped the reaction, discharged excess ethylene gas, separated the lower organic layer, washed with water, washed with saturated salt, dried with anhydrous sodium sulfate, and removed the organic solvent under vacuum to obtain the compound perfluorooctane ethyl iodine is a white solid (525g, yield 95%, mp56-57 ℃). KOH(7.0g, 0.1mol) and methyl 30mL were added to a 250mL three-mouth flask equipped with a reflux condenser tube, a dropping funnel and a thermometer. The compound perfluorooctane ethyl iodine (47.4g, 0.1mol) was dissolved in 100mL Freon-113 solvent, and then the solution was slowly added dropwise into the methanol solution of KOH. The reaction is exothermic and a large amount of solid is generated. After dropping, heat and reflux for 3 hours. The reaction mixture was poured into 250mL of water, the organic layer was separated, dried with anhydrous Na2SO4 and distilled to obtain the compound perfluorooctylethylene (28.0g, yield 81%).

Last Update：2024-04-10 22:29:15

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1H,1H,2H-PERFLUORO-1-DECENE

1H,1H,2H-PERFLUORO-1-DECENE

3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodec-1-ene

CAS: 21652-58-4

Molecular Formula: C10H3F17

1H,1H,2H-PERFLUORO-1-DECENE - Names and Identifiers

1H,1H,2H-PERFLUORO-1-DECENE - Physico-chemical Properties

1H,1H,2H-PERFLUORO-1-DECENE - Risk and Safety

1H,1H,2H-PERFLUORO-1-DECENE - Reference Information

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3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodec-1-ene

CAS: 21652-58-4

Molecular Formula: C10H3F17

1H,1H,2H-PERFLUORO-1-DECENE - Names and Identifiers

1H,1H,2H-PERFLUORO-1-DECENE - Physico-chemical Properties

1H,1H,2H-PERFLUORO-1-DECENE - Risk and Safety

1H,1H,2H-PERFLUORO-1-DECENE - Reference Information

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1H,1H,2H-PERFLUORO-1-DECENE