Name | 2'-Benzoylacetanilide |
Synonyms | 2-Benzoylacatanilide 2'-Benzoylacetanilide acetamido-2benzophenone 2-ACETAMINOBENZOPHENONE 2-(Acetylamino)benzophenone n-(2-benzoylphenyl)-acetamid |
CAS | 85-99-4 |
Molecular Formula | C15H13NO2 |
Molar Mass | 239.27 |
Density | 1.1198 (rough estimate) |
Melting Point | 87 °C |
Boling Point | 381.93°C (rough estimate) |
pKa | 14.54±0.70(Predicted) |
Refractive Index | 1.5500 (estimate) |
Physical and Chemical Properties | White foliate crystals. Melting point 108 ℃. Soluble in ethanol, chloroform, hot benzene and alkali solution, slightly soluble in water and benzene. |
Hazard Symbols | Xi - Irritant |
Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
Safety Description | S37/39 - Wear suitable gloves and eye/face protection S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. |
WGK Germany | 2 |
RTECS | AB4542950 |
uses | organic synthesis intermediates, analytical reagents. |
Production method | It is obtained by the reaction of ethyl benzoyl acetate and aniline. Heat ethyl benzoylacetate and anhydrous xylene together to 150 ℃, stir and add aniline dropwise, while reacting, while distilling the produced ethanol, the reaction ends when the ethanol is no longer distilled. Crystallize the reactants in petroleum ether, filter, wash, and then recrystallize with benzene to obtain the product. The yield is about 75%. |