2-Nitrofluorene
2-Nitrofluorene
CAS: 607-57-8
Molecular Formula: C13H9NO2
2-Nitrofluorene - Names and Identifiers
| Name | 2-Nitrofluorene |
| Synonyms | 2-Nitrof NSC 5182 HSDB 2111 AI3-08839 CCRIS 1189 BRN 1877983 Nitrofluorene 2-NITROFLUORENE 2-Nitrofluorene 2-NITROFLUOROENE 2-nitro-9h-fluoren Fluorene, 2-nitro- 2-Nitro-9H-fluorene 9H-Fluorene, 2-nitro- 4-05-00-02149 (Beilstein Handbook Reference) |
| CAS | 607-57-8 |
| EINECS | 210-138-5 |
| InChI | InChI=1/C13H9NO2/c15-14(16)11-5-6-13-10(8-11)7-9-3-1-2-4-12(9)13/h1-6,8H,7H2 |
2-Nitrofluorene - Physico-chemical Properties
| Molecular Formula | C13H9NO2 |
| Molar Mass | 211.22 |
| Density | 1.1868 (rough estimate) |
| Melting Point | 156-158 °C (lit.) |
| Boling Point | 350.9°C (rough estimate) |
| Flash Point | 185.2°C |
| Water Solubility | Insoluble |
| Vapor Presure | 1.77E-05mmHg at 25°C |
| Appearance | Powder |
| Color | White to brown |
| Storage Condition | Keep in dark place,Sealed in dry,Room Temperature |
| Stability | Stable. Incompatible with strong oxidizing agents. |
| Refractive Index | 1.6060 (estimate) |
| Physical and Chemical Properties | Yellow needle-like crystals. Melting point 156 °c. |
2-Nitrofluorene - Risk and Safety
| Risk Codes | R40 - Limited evidence of a carcinogenic effect R51/53 - Toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. R68 - Possible risk of irreversible effects |
| Safety Description | S36/37 - Wear suitable protective clothing and gloves. S61 - Avoid release to the environment. Refer to special instructions / safety data sheets. |
| UN IDs | UN 3077 9/PG 3 |
| WGK Germany | 3 |
| RTECS | LL8225000 |
| TSCA | Yes |
| HS Code | 29042000 |
| Hazard Class | 9 |
| Packing Group | III |
2-Nitrofluorene - Reference Information
| (IARC) carcinogen classification | 2B (Vol. 46, 105) 2014 |
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| use | organic synthesis intermediate. |
| production method | 60g fluorene and 500ml glacial acetic acid are mixed evenly, stirred and heated to 50 ℃, and 80ml concentrated nitric acid is added dropwise. React at 80 ℃ for 5min, cool to room temperature, filter out the generated 2-nitrofluorene, wash with cold glacial acetic acid, and recrystallize with glacial acetic acid to obtain 56g of pure product with 79% yield. |
| toxic substance data | information provided by: pubchem.ncbi.nlm.nih.gov (external link) |
Last Update：2024-04-10 22:29:15
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