208665-96-7
3-bromo-4-isobutoxy-benzenecarbothioamide
CAS: 208665-96-7
Molecular Formula: C11H14BrNOS
208665-96-7 - Names and Identifiers
| Name | 3-bromo-4-isobutoxy-benzenecarbothioamide |
| Synonyms | Bromo-4-isobutoxybenzothioamide 3-bromo-4-isobutoxythiobenzamide 3-Bromo-4-isobutoxybenzothioamide 3-bromo-4-isobutoxyphenylthiocarboxamide 3-Bromo-4-isobutoxybenzenecarbothioamide 3-bromo-4-isobutoxy-benzenecarbothioamide Benzenecarbothioamide, 3-bromo-4-(2-methylpropoxy)- benzenecarbothioamide, 3-bromo-4-(2-methylpropoxy)- 3-broMo-4-(2-Methylpropoxy)benzene-1-carbothioaMide |
| CAS | 208665-96-7 |
| InChI | InChI=1/C11H14BrNOS/c1-7(2)6-14-10-4-3-8(11(13)15)5-9(10)12/h3-5,7H,6H2,1-2H3,(H2,13,15) |
208665-96-7 - Physico-chemical Properties
| Molecular Formula | C11H14BrNOS |
| Molar Mass | 288.2 |
| Density | 1.398g/cm3 |
| Boling Point | 370.783°C at 760 mmHg |
| Flash Point | 178.043°C |
| Vapor Presure | 0mmHg at 25°C |
| Refractive Index | 1.602 |
208665-96-7 - Introduction
It is an organic compound with the molecular formula C12H15BrNOS.
Nature:
-Appearance: Colorless or pale yellow crystalline solid.
-Solubility: Soluble in some organic solvents, such as chloroform, dichloromethane and ethanol, insoluble in water.
-Melting point: about 83-86 ° C.
Use:
-is an organic compound synthesis intermediate, widely used in drug synthesis, fungicide synthesis and other fields.
Method:
The preparation method can be carried out by the following steps:
1. P-Hydroxybenzenesulfonylthionyl chloride (compound A) is reacted with 3-bromoisobutanol to give 3-bromo-4-isobutyrylbenzenesulfonylthionyl chloride (compound B).
2. React compound B with ammonia water to generate.
Safety Information:
-is a chemical reagent that requires personal protective measures such as gloves, goggles and protective clothing.
-When using or handling, avoid inhaling its dust or solution, and try to avoid skin contact.
-In case of contact with skin or eyes, rinse immediately with plenty of water.
-When storing, it should be stored in a closed container to avoid contact with oxygen, fire sources and strong oxidants to avoid fire or explosion.
Nature:
-Appearance: Colorless or pale yellow crystalline solid.
-Solubility: Soluble in some organic solvents, such as chloroform, dichloromethane and ethanol, insoluble in water.
-Melting point: about 83-86 ° C.
Use:
-is an organic compound synthesis intermediate, widely used in drug synthesis, fungicide synthesis and other fields.
Method:
The preparation method can be carried out by the following steps:
1. P-Hydroxybenzenesulfonylthionyl chloride (compound A) is reacted with 3-bromoisobutanol to give 3-bromo-4-isobutyrylbenzenesulfonylthionyl chloride (compound B).
2. React compound B with ammonia water to generate.
Safety Information:
-is a chemical reagent that requires personal protective measures such as gloves, goggles and protective clothing.
-When using or handling, avoid inhaling its dust or solution, and try to avoid skin contact.
-In case of contact with skin or eyes, rinse immediately with plenty of water.
-When storing, it should be stored in a closed container to avoid contact with oxygen, fire sources and strong oxidants to avoid fire or explosion.
Last Update：2024-04-09 02:00:44
