29713-15-3
1,3-Adamantanedicarbonyl dichloride
CAS: 29713-15-3
Molecular Formula: C12H14Cl2O2
29713-15-3 - Names and Identifiers
| Name | 1,3-Adamantanedicarbonyl dichloride |
| Synonyms | 1,3-Adamantanedicarbonyl chloride adamantane-1,3-dicarbonyl chloride 1,3-Adamantanedicarbonyl dichloride Tricyclo[3.3.1.13,7]decane-1,3-dicarbonyl dichloride tricyclo[3.3.1.1~3,7~]decane-1,3-dicarbonyl dichloride |
| CAS | 29713-15-3 |
| InChI | InChI=1/C12H14Cl2O2/c13-9(15)11-2-7-1-8(4-11)5-12(3-7,6-11)10(14)16/h7-8H,1-6H2 |
29713-15-3 - Physico-chemical Properties
| Molecular Formula | C12H14Cl2O2 |
| Molar Mass | 261.14 |
| Density | 1.441 |
| Melting Point | 89-90 °C |
| Boling Point | 318°C at 760 mmHg |
| Flash Point | 161°C |
| Vapor Presure | 0.000372mmHg at 25°C |
| Refractive Index | 1.586 |
29713-15-3 - Introduction
1,3-adamantanedicarbonyl dichloride, also known as 1,3-adamantanedicarbonyl dichloride, is an organic compound. It has a chemical formula of CIS and a molecular weight of 287.16g/mol.
1,3-adamantanedicarbonyl dichloride is a colorless to light yellow liquid, stable at room temperature. It has a strong pungent odor and is soluble in a variety of organic solvents.
1,3-adamantanedicarbonyl dichloride is mainly used as an important reagent and intermediate in organic synthesis. It can be used to synthesize compounds containing 1,3-adamantane diformyl groups, such as adamantane diformyl amide, adamantane diformyl imide and adamantane diformyl ketone. These compounds have a wide range of applications in the fields of medicine and materials science.
The method for preparing 1,3-adamantanedicarbonyl dichloride can be obtained by reacting adamantanedione and thionyl chloride. First, the adamantanedione and thionyl chloride are heated to reflux under the protection of nitrogen, and then the reaction mixture is cooled to room temperature, the solvent and unreacted adamantanedione are separated, and finally the desired 1 is extracted by distillation, 3-Adamantanedicarbonyl dichloride product.
When using 1,3-adamantanedicarbonyl dichloride, it is necessary to pay attention to its irritation to the skin and eyes, and appropriate personal protective measures should be taken. It should also be stored in a dry, cool place, away from fire and oxidizing agents. In addition, due to its pungent odor, it should be operated in a well-ventilated environment. Seek immediate medical help if large amounts of 1,3-adamantanedicarbonyl dichloride are inhaled or exposed.
1,3-adamantanedicarbonyl dichloride is a colorless to light yellow liquid, stable at room temperature. It has a strong pungent odor and is soluble in a variety of organic solvents.
1,3-adamantanedicarbonyl dichloride is mainly used as an important reagent and intermediate in organic synthesis. It can be used to synthesize compounds containing 1,3-adamantane diformyl groups, such as adamantane diformyl amide, adamantane diformyl imide and adamantane diformyl ketone. These compounds have a wide range of applications in the fields of medicine and materials science.
The method for preparing 1,3-adamantanedicarbonyl dichloride can be obtained by reacting adamantanedione and thionyl chloride. First, the adamantanedione and thionyl chloride are heated to reflux under the protection of nitrogen, and then the reaction mixture is cooled to room temperature, the solvent and unreacted adamantanedione are separated, and finally the desired 1 is extracted by distillation, 3-Adamantanedicarbonyl dichloride product.
When using 1,3-adamantanedicarbonyl dichloride, it is necessary to pay attention to its irritation to the skin and eyes, and appropriate personal protective measures should be taken. It should also be stored in a dry, cool place, away from fire and oxidizing agents. In addition, due to its pungent odor, it should be operated in a well-ventilated environment. Seek immediate medical help if large amounts of 1,3-adamantanedicarbonyl dichloride are inhaled or exposed.
Last Update：2024-04-09 21:04:16
