29964-62-3
Bisdiphenylphosphinobutanepalladiumdichloride
CAS: 29964-62-3
Molecular Formula: C28H28Cl2P2Pd
29964-62-3 - Names and Identifiers
| Name | Bisdiphenylphosphinobutanepalladiumdichloride |
| Synonyms | Bisdiphenylphosphinobutanepalladiumdichloride 1,4-Bis(diphenylphosphino)butane-palladium(II)chloride 1,4-Bis(diphenylphosphino)butane-palladium(II) chloride [1,4-Bis(diphenylphosphino)butane]palladium(II) dichloride |
| CAS | 29964-62-3 |
| InChI | InChI=1/C28H28P2.2ClH.Pd/c1-5-15-25(16-6-1)29(26-17-7-2-8-18-26)23-13-14-24-30(27-19-9-3-10-20-27)28-21-11-4-12-22-28;;;/h1-12,15-22H,13-14,23-24H2;2*1H;/q;;;+2/p-2 |
29964-62-3 - Physico-chemical Properties
| Molecular Formula | C28H28Cl2P2Pd |
| Molar Mass | 603.8 |
| Melting Point | 213℃ |
| Boling Point | 542°C at 760 mmHg |
| Flash Point | 299.5°C |
| Vapor Presure | 2.92E-11mmHg at 25°C |
| Appearance | Yellow solid |
| Storage Condition | Room Temprature |
| MDL | MFCD02093437 |
| Use | Metal organic catalysts. It is widely used in organic synthesis. |
29964-62-3 - Introduction
A radical, also known as a radical, is an organometallic compound. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
is a yellow to yellow-orange crystal, soluble in organic solvents such as chloroform, dimethylformamide, etc. It is a complex containing two 1,4-biphenylphosphine ligands and two chloride ligands.
Use:
It is widely used as a catalyst in organic synthesis reactions. It can be used in the coupling reaction of aniline and ketene to generate substituted enamine derivatives. In addition, it can also be used for other types of cross-coupling reactions, reduction reactions, and cyclization reactions.
Method:
The method of preparing phosphonium is usually to react phenyldichlorophosphine and hexanedione with palladium chloride in an appropriate solvent. The reaction is usually carried out under an inert atmosphere, and the reaction solvent is usually methyl chloride or benzyl chloride.
Safety Information:
Toxicity and safety data are relatively limited. Due to its chlorine-containing ligand, it may be somewhat toxic to the environment. Wear appropriate protective equipment, including safety glasses and chemical protective gloves. In addition, proper laboratory safety practices need to be followed during use.
Nature:
is a yellow to yellow-orange crystal, soluble in organic solvents such as chloroform, dimethylformamide, etc. It is a complex containing two 1,4-biphenylphosphine ligands and two chloride ligands.
Use:
It is widely used as a catalyst in organic synthesis reactions. It can be used in the coupling reaction of aniline and ketene to generate substituted enamine derivatives. In addition, it can also be used for other types of cross-coupling reactions, reduction reactions, and cyclization reactions.
Method:
The method of preparing phosphonium is usually to react phenyldichlorophosphine and hexanedione with palladium chloride in an appropriate solvent. The reaction is usually carried out under an inert atmosphere, and the reaction solvent is usually methyl chloride or benzyl chloride.
Safety Information:
Toxicity and safety data are relatively limited. Due to its chlorine-containing ligand, it may be somewhat toxic to the environment. Wear appropriate protective equipment, including safety glasses and chemical protective gloves. In addition, proper laboratory safety practices need to be followed during use.
Last Update：2024-04-09 21:04:16
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