Molecular Formula | C6H6Br2N2O2S |
Molar Mass | 330 |
Density | 2.156±0.06 g/cm3(Predicted) |
Melting Point | 235-237°C |
Boling Point | 458.2±55.0 °C(Predicted) |
Storage Condition | RT, dark |
MDL | MFCD00014783 |
Physical and Chemical Properties | Chemical properties white crystal. Melting point 236-238 ℃. |
Use | Uses intermediates in organic synthesis. |
Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36 - Wear suitable protective clothing. |
Raw Materials | Hydrogen peroxide Sulfanilamide |
dissolve p-aminobenzenesulfonamide in hydrobromic acid aqueous solution, heat to 70-75 ℃, and add 30% hydrogen peroxide. The reaction is exothermic, and the temperature rises to 85-90°C. When stirring the reaction, the reactants almost become solids. Suction and filtration while hot to obtain 3, 5-dibromop-aminobenzenesulfonamide with a yield of 90-94%.
storage conditions | Keep in dark place,Inert atmosphere,Room temperature |
acidity coefficient (pKa) | 9.57±0.60(Predicted) |