31301-31-2 - Names and Identifiers
31301-31-2 - Physico-chemical Properties
Molecular Formula | C14H8N2O4
|
Molar Mass | 268.22 |
Density | 1.585 |
Melting Point | >300℃ |
Storage Condition | Sealed in dry,Room Temperature |
31301-31-2 - Introduction
1,10-phenanthroline-4, 7-dicarboxylic acid is an organic compound with the chemical formula C14H8N2O4. The following is a description of its nature, use, formulation and safety information:
Nature:
-Appearance: 1,10-phenanthroline-4, 7-dicarboxylic acid is a pale yellow crystalline solid.
-Solubility: It has a low solubility in water, but it can be dissolved in some organic solvents, such as ethanol and dimethylformamide.
-Thermal stability: Its melting point is about 226-230 ℃, which can be stable at this temperature.
Use:
-Coordination reagent: 1,10-phenanthroline-4, 7-dicarboxylic acid is a ligand with large coordination ability, which is often used in coordination chemistry research and catalytic reactions.
-Analytical chemistry: It can be used as a reagent for the determination and analysis of metal ions.
-Optics: Due to its structurally constrained molecular configuration, 1,10-phenanthroline-4, 7-dicarboxylic acid can be used as a template for preparing two-dimensional complex structures.
Method:
There are many ways to prepare 1,10-phenanthroline-4, 7-dicarboxylic acid. The commonly used methods include the following steps:
1. First, 1,10-biphenanthroline was synthesized from the acylation reaction between catechol and nitroacetophenone;
2. Then 1,10-Phenanthroline is reacted with sodium cyanide and dimethyl sulfoxide to generate 1,10-phenanthroline-4, 7-dicarboxylic acid through acid-catalyzed nitrilization.
Safety Information:
-1,10-phenanthroline-4, 7-dicarboxylic acid has low toxicity, but it still needs to be handled carefully.
-Avoid direct contact with skin and eyes during operation.
-Avoid fire and high temperature during storage and handling.
-During use, please be equipped with appropriate personal protective equipment, such as laboratory gloves, goggles, etc.
-Do not mix it with strong oxidants or strong acids to avoid dangerous reactions.
Last Update:2024-04-10 22:29:15