5-bromo-1,10-phenanthroline

Name	5-bromo-1,10-phenanthroline
Synonyms	FFC 5-Bromo-1,1-phenanthroline 5-Bromo-1,10-phenanthroline 5-bromo-1,10-phenanthroline 1,10-Phenanthroline, 5-bromo- 1,10-Phenanthroline, 5-broMo- 5-bromo-1,10-phenanthroline, Fandachem
CAS	40000-20-2
EINECS	254-742-7
InChI	InChI=1/C12H7BrN2/c13-10-7-8-3-1-5-14-11(8)12-9(10)4-2-6-15-12/h1-7H

Molecular Formula	C12H7BrN2
Molar Mass	259.1
Density	1.616
Melting Point	119°C(lit.)
Boling Point	417.6±25.0 °C(Predicted)
Flash Point	206.3°C
Vapor Presure	8.5E-07mmHg at 25°C
Appearance	powder to crystal
Color	White to Light yellow to Light orange
pKa	3.98±0.10(Predicted)
Storage Condition	Keep in dark place,Sealed in dry,Room Temperature
Refractive Index	1.757

EPA chemical information	Information provided by: ofmpub.epa.gov (external link)
use	5-bromo-1, 10-phenanthroline can be used in organic synthesis intermediates and pharmaceutical intermediates, and can be used in laboratory research and development processes and chemical and pharmaceutical synthesis processes.
preparation	preparation of 5-bromo -1,10-phenanthroline: 22.31g(100mmol) of 5-bromo -8-quinoline amine (Y), 7.61g(100mmol) of 1,3-propylene glycol, 1.12g(5mmol) of palladium acetate, 1.21g(5mmol)2,4, 6-Trimethylpyridine, 1.14g(10mmol) trifluoroacetic acid, in oxygen atmosphere (1atm), the temperature was raised to 150 ℃, and the reaction was carried out for 12 hours. After the reaction is over, the filtrate is filtered, concentrated, and purified by column chromatography to obtain the intermediate 5-bromo-1, 10-phenanthroline.

Last Update：2024-04-10 22:29:15

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CAS: 40000-20-2
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5-bromo-1,10-phenanthroline

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