51889-44-2
n-Octylferrocene
CAS: 51889-44-2
Molecular Formula: C18H26Fe
51889-44-2 - Names and Identifiers
| Name | n-Octylferrocene |
| Synonyms | Octylferrocene n-Octylferrocene Cyclopentadienyl(octylcyclopentadienyl)-iron |
| CAS | 51889-44-2 |
51889-44-2 - Physico-chemical Properties
| Molecular Formula | C18H26Fe |
| Molar Mass | 298.24 |
| Storage Condition | Room Temprature |
51889-44-2 - Reference Information
| application | n-octyl ferrocene is a ferrocene derivative. The structure of non-benzene aromatic ring metal organic compounds of ferrocene and its derivatives makes them have very special properties, and can be used in fuel oil fuel-saving smoke inhibitors, gas combustion catalysts, ultraviolet absorbers, photosensitive catalysts, Various drugs, biological enzyme electrodes and other fields. |
| preparation | a mixed solvent recrystallization method for efficient preparation of high purity n-octyl ferrocene, characterized by the following steps: step 1: the crude n-octyl ferrocene, polar protic solvent containing hydroxyl group, polar aprotic solvent and non-polar solvent are prepared in a volume ratio of 1:4 to 5:4 to 5:8 to 10; Step 2: After the prepared solution is placed at a temperature of -10 ℃ to -80 ℃ to precipitate n-octyl ferrocene crystals, pour out the 50% solvent and filter to obtain n-octyl ferrocene crystals; replace the crude n-octyl ferrocene in step 1 with the n-octyl ferrocene crystal this time, and repeat steps 1 to 2 six times; step 3: place the crystals collected after repeated six times in a vacuum oven at a temperature of 40~60 ℃ and a relative vacuum degree of -0.05 ~-0.08Mpa. after 3~4 hours, nitrogen is filled until the internal and external pressures are equal, the vacuum is pumped to -0.05 ~-0.08Mpa, then nitrogen is filled, and the process of filling nitrogen to vacuuming is repeated for 8~10 times to obtain high purity n-octyl ferrocene. |
Last Update：2024-04-09 21:04:16
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