536-80-1
Iodosylbenzene
CAS: 536-80-1
Molecular Formula: C6H5IO
536-80-1 - Names and Identifiers
| Name | Iodosylbenzene |
| Synonyms | IODOSOBENZENE iodosobenzene iodoso-benzen Iodosylbenzene iodosyl-benzen Benzene, iodosyl- phenyliodane oxide Phenyloxoiodine(III) [Oxoiodo(III)]benzene Phenyliodine(III) oxide 4-05-00-00692 (Beilstein Handbook Reference) |
| CAS | 536-80-1 |
| EINECS | 208-648-8 |
| InChI | InChI=1/C6H5IO/c8-7-6-4-2-1-3-5-6/h1-5H |
| InChIKey | JYJVVHFRSFVEJM-UHFFFAOYSA-N |
536-80-1 - Physico-chemical Properties
| Molecular Formula | C6H5IO |
| Molar Mass | 220.01 |
| Density | 1.8665 (estimate) |
| Melting Point | 210°C (rough estimate) |
| Water Solubility | Slightly soluble in water |
| Solubility | Soluble in water, and methanol. |
| Appearance | powder to crystal |
| Color | White to Yellow to Green |
| Merck | 14,5044 |
| Storage Condition | Freezer |
| Sensitive | Sensitive to heat and light |
| MDL | MFCD00039507 |
536-80-1 - Risk and Safety
| Safety Description | S17 - Keep away from combustible material. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. |
| UN IDs | 1479 |
| RTECS | DA3500000 |
| HS Code | 29039990 |
| Hazard Class | 4.1 |
| Packing Group | II |
536-80-1 - Reference Information
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| production method | 32.2g(0.10mol) of iodide benzene diacetate is placed in a 250ml beaker, and 150ml of 3mol/L sodium hydroxide solution is added within 5min under vigorous stirring. Grind the resulting solid mass with a stirring rod or spoon for 15min, and leave the reaction mixture for another 45min to complete the reaction. Add 100ml of water, vigorously stir the mixture, and collect solid crude iodionyl benzene on the Brinell funnel. Return the wet solid to the beaker and break it in 200ml of water. Collect the solids in a cloth funnel, wash with 200ml of water, and suck and filter until dry. Finally, when delicate, break the dry solid in a beaker in 75ml chloroform. Iodine benzene was filtered out and dried in air to obtain 18.7~20.5g(85% ~ 93%) and mp210 ℃. |
Last Update：2024-04-09 02:00:09
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